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  • 1
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Magnetic properties of Fe3Si films with thickness from 2 to 210 monolayers (ML) epitaxially grown on GaAs (001) were studied using a superconducting quantum interference device and alternating gradient force magnetometers. Growth of these single-crystal intermetallic compound films were carried out in a multichamber molecular beam epitaxy (MBE) system. The samples were covered in situ with Au 50 A(ring) thick to prevent oxidation when the samples were removed from the MBE chamber. All the films are ferromagnetic even for samples as thin as 2 ML. The easy magnetization direction of the films is parallel to the film surface. The magnetic coercivity forces (Hc) of the samples increase as the film thickness decreases to 10 ML, and then decrease when the film thickness decreases further to 2 ML.
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 6872-6879 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The magnitude of the stress in a thin film can be obtained by measuring the curvature of the film–substrate couple. Crystal curvature techniques yield the average stress throughout the film thickness. On a microscopic level, the details of the strain distribution, as a function of depth through the thickness of the film, can have important consequences in governing film quality and ultimate morphology. A new method, using high-resolution x-ray diffraction to determine the depth dependence of strain in polycrystalline thin films, is described. The technique requires an analysis of the diffraction peak shifts of at least six independent {hkl} scattering vectors, at a variety of penetration depths from the free surface of the film. The data are then used to determine the magnitude and directions of the strain eigenvalues in a laboratory reference frame for each penetration depth from the free surface of the film. A linear elastic model was used to determine the strains in successive slabs of the film. Results are reported for two Mo films, with nominal thicknesses of 50 and 100 nm, which were deposited by planar magnetron sputtering onto Si (100) substrates. This technique can provide quantitative insight into the depth variation of residual strains (stresses) in thin films and should work with a wide variety of materials. © 1996 American Institute of Physics.
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 5060-5062 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We have prepared nanometer-size, isolated CoPt particles. The particles in the range of 100–300 nm in diameter were formed by annealing thin films in the temperature range of 550–800 °C. Films with magnetic coercivity as high as 30 kOe were achieved. The results indicate that the high magnetic coercivity was obtained because the crystallite size approaches that of noninteracting single-domain particles. © 1996 American Institute of Physics.
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 5958-5960 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Rare earth–cobalt (RCo, R=Sm, Pr) films with thicknesses from 30 to 700 nm have been prepared with and without a Cr underlayer by dc magnetron sputtering from a R2Co7 composite target. The as-deposited SmCo films with a Cr underlayer (SmCo(parallel)Cr) have magnetic coercivities of about 500–2800 Oe and the PrCo(parallel)Cr films have coercivities of about 100–300 Oe, but after annealing at 500 °C coercivities as high as 31 kOe for SmCo(parallel)Cr films and 10 kOe for PrCo(parallel)Cr films were observed. The as-deposited PrCo films are composed mostly of an amorphous phase with about 30 vol % of crystallites but after annealing at 500 °C the film is transformed completely to crystallites of about 10 nm diameter as revealed by high-resolution transmission electron microscopy (HRTEM). Nanodiffraction and HRTEM studies show that the crystallites have a closed-packed hexagonal structure. HRTEM study also shows that the annealed SmCo films with a Cr underlayer have grain sizes of about 20 nm and the SmCo films without the Cr underlayer have grain sizes of about 10 nm. The large increase in coercivity for the annealed films is due to the growth of the crystallites. © 1996 American Institute of Physics.
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 79 (1996), S. 6448-6450 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: We report on magnetic force microscopy (MFM) images of a thin-film magnetic recording head taken using batch micromachined silicon tips coated with nanocomposite Fe60(SiO2)40 and Fe70(SiO2)30 films. The small Fe grain size (〈10 nm) and dilute Fe volume fraction (0.29–0.4) of these granular films produce tip coatings of low remanence and essentially zero coercivity, reduced by the superparamagnetic properties of these films. We have used these tips to obtain MFM images of the write field of the head with high spatial and magnetic-field resolution. In comparison to images taken using commercial Co85Cr15-coated tips, these MFM images show reduced tip memory effects and clearly delineate the gap field from the pole pieces. © 1996 American Institute of Physics.
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  • 6
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 73 (1993), S. 5539-5539 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Recently a great deal of attention has been focused on giant magnetoresistance (GMR), especially in the coupled multilayer magnetic films. In this report, we show that GMR also exists in nanocomposite films. We have systematically studied the magnetoresistance of Fe/Ag and Co/Ag nanocomposite films with 15 to 55 at. % of Fe and Co, respectively. These films were prepared by magnetron sputtering from composite targets. The crystallite size of the Fe and Co are from 30 to 150 A(ring) which was controlled by the substrate temperature and determined by the analysis of the x-ray diffraction patterns. All samples have a negative magnetoresistance and the change of magnetoresistance varies from a fraction of a percent to more than 25% at 6 K and under 5 Tesla magnetic field. We have investigated the effect of the particle size and particle separation distance on the magnetoresistance and their magnetic properties will be presented.
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  • 7
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Nanocomposite Fe80(SiO2)20 films with thickness from 150 to 5000 A(ring) have been prepared by rf magnetron sputtering from a composite target. The crystallites in the Fe80(SiO2)20 films have a bcc structure with the average size of 46–66 A(ring) which was determined by transmission electron microscopy. As indicated by the thickness dependence of resistivity, the stacking and connectivity of the crystallites depend on the thickness of the films. The magnetic properties also depend on the microstructure which changes with the thickness of the films. The magnetic coercivity of the films increases with the thickness of the film, reaches a maximum, and then decreases. The maximum coercivity of 400 Oe at 300 K and 1200 Oe at 5 K was observed for a film with a thickness of about 700 A(ring).
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  • 8
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Nanostructured Co/Ag composite films were prepared by magnetron sputtering using a single target. The average crystallite sizes of Co and Ag in the films depend on the deposition conditions. As the substrate temperature increases from 100 °C to 600 °C, the average Ag crystallite size increases from 39 to 452 A(ring), and the average Co crystallite size increases from 〈30 to 297 A(ring) in the film with 39 vol. % of Co. The films with 39 vol. % of Co and prepared at 400 °C substrate temperature showed a maximum magnetic coercivity of 565 Oe at 6 K. We have studied the correlation between the structure and magnetic properties of these films.
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  • 9
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 78 (2001), S. 904-906 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Electromigration in 0.27 μm wide Cu damascene interconnections has been investigated. The results show that the electromigration time to failure of Cu interconnections is greatly influenced by the thickness of the metal liner at the contact between the via and underlying line. A remarkably long lifetime was achieved when a 3 nm thick liner (at the via/metal line interface) was used, since the abrupt mass flux divergence at this interface normally seen is greatly diminished. Voids were found in the regions where there was no electric field and on the bamboo Cu grain structure. Void formation is explained by the effect of a vacancy wind. © 2001 American Institute of Physics.
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  • 10
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: CoSm films with a Cr underlayer (CoSm//Cr) are promising as future high density recording media.1 It was pointed out that the grain size in media affects the media noise and thermal stability significantly. However, if small grains are exchange coupled to form larger "magnetic grains," the size of these magnetic clusters will be important in noise considerations. Our previous works23 indicated that for CoSm film with Cr underlayer the magnetic grain size is much larger than the 50 Å nanocrystallites and is about the same size as the Cr grain of ∼240 Å in dimension. In the present work, we report our systematic studies of magnetic switching volume and its correlation with magnetic and nanostructural properties for CoSm films. Switching volumes V* were measured with the "field sweep-rate dependence of coercivity Hc," interactions among the magnetic grains were estimated with the so-called ΔM method, and the nanostructures were investigated with atomic force microscopy and transmission electron microscopy. The thickness of CoSm layers, which were sputtered in an Ar pressure PAr=25 mT, is 300 Å for all samples. It is found that as the Cr underlayer thickness dCr increases from 0 Å (without a Cr underlayer) to 200 Å, the V* and ΔMmax decrease (Hc increases) rapidly, i.e., from V* from 9.3×10−18 to 5.7×10−18 cm3, ΔMmax from 1.3 to 0.5 (Hc from 1.4 to 2.3 kOe), respectively, and then gradually as dCr approaches 800 Å. As Ar pressure PAr of the deposition of the Cr underlayer varies from 5 to 30 mT, the V* and ΔMmax have their minima (anisotropy Ku has its maximum) at PAr(similar, equals)9.5 mT. V* shows minima at dCr and PAr values where Hc and Ku have their maxima and ΔMmax has a small value. This behavior can be interpreted with a thermal activation model including interactions between magnetic grains. The relationship between crystallite grain size, magnetic grain V*, and media noise will be discussed. ©1997 American Institute of Physics.
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