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  • 1
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A high-energy double-crystal x-ray monochromator has been constructed for use on the X-17 beam line at the National Synchrotron Light Source (NSLS). Its design is based on the "boomerang'' right angle linkage, and features a fixed exit beam, a cooled first crystal, and an energy range of 8–92 keV. The entire mechanism is UHV compatible. The design is described and performance details, obtained in testing at the X17 beam line, are presented.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 73 (2002), S. 1509-1509 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A fixed-exit double crystal monochromator based on one rotation has been designed for an absorption spectroscopy beamline. The first crystal is mounted in the center of rotation, while the second crystal is translated by simple mechanical means. This change of the gap distance d keeps the beam offset constant. The second crystal is tuned by a simple digital feedback system, which allows us to control both θ and χ. The first crystal is mounted in the center of rotation to improve its cooling compared to the existing boomerang design, which only allows indirect cooling. In the present design, the cooling lines are fixed on the circle and are moved together with the crystal, so that no additional force acts on the crystal. The monochromator has been tested between 5 and 11 keV for the Si(111) reflection and between 6.5 and 8 keV for the Si(333) reflection. The beam motions were less than 300 μm with the mechanism not optimized. Measurements of the Cu K edge extended x-ray absorption fine structure in CuO gave the same result as from a conventional double crystal channel-cut crystal. See J. A. Golovchenko, R. A. Levesque, and P. L. Cowan, Rev. Sci. Instrum. 52, 509 (1981). © 2002 American Institute of Physics.
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 73 (2002), S. 1510-1510 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A polarization analyzer has been designed for soft x-ray resonant diffraction experiments at the S K edge. The Bragg angle of graphite (0001) at the S K edge is 48°, which makes it perfectly suited as polarization analyzer. Two graphite (0001) crystals (12×12×2 mm3) are mounted on small tangent-arm driven spring loaded stages with their diffraction planes in the horizontal and vertical plane for σ and π analysis of polarized x rays. The diffracted x rays are detected by small peltier cooled Si detectors with dimensions 1×12 mm2 with the longer dimension in the direction of diffraction, so that the detector can remain fixed. These two polarization analyzers and an additional detector for the directly diffracted beam are mounted on a stage, so that the polarization of the diffracted x rays can be determined just by moving the appropriate analyzer into the beam. The tangent arm and the detector allow us to scan ±50 eV around the S K edge. This setup avoids mounting of the polarization analyzer on a rotation stage, whose axis has to be aligned with the diffracted beam. The tangent-arm is driven by motorized micrometers, which are equipped with encoders to obtain an angular resolution of 0.001°. © 2002 American Institute of Physics.
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  • 4
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Silicon crystals at room temperature employed as x-ray monochromators on synchrotron radiation beamlines, when subjected to high-power-density loading, suffer thermal distortions which compromise their x-ray diffraction efficiency and result in a reduction of the inherent brilliance of the synchrotron beam. At cryogenic temperatures however (below 150 K), silicon crystals suffer little or no thermal distortions under high-power-density loading. The design and implementation of a channel-cut silicon crystal monochromator which is cooled to as low as 50 K, using a commercial helium refrigerator and circulation system and a custom-designed heat exchanger for the monochromator crystal, are described. Test results have been obtained on the National Synchrotron Light Source X13B in-vacuum undulator beamline as well as the higher power X25 wiggler beamline. © 2002 American Institute of Physics.
    Type of Medium: Electronic Resource
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