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  • Wiley-Blackwell  (2)
  • 1965-1969  (2)
  • 1
    ISSN: 0449-2951
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: A dye partition method for the determination of hydroxyl endgroups in poly(methyl methacrylate) samples prepared in aqueous media with the use of hydrogen peroxide as the photoinitiator has been described. The dried polymers were treated with chlorosulfonic acid under suitable conditions whereby the hydroxyl endgroups present in them were transformed to sulfate endgroups. Spectrophotometric analysis of sulfate endgroups in the treated polymers was carried out by the application of the dye-partition technique developed for the purpose, and thus a measure of hydroxyl endgroups in the original polymers was obtained. H2O2, in the concentration range of 0.004-0.1M, was found to incorporate an average of nearly 1 OH endgroup per polymer chain.
    Additional Material: 1 Tab.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 11 (1967), S. 1603-1611 
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Graft copolymerization of natural rubber and MMA was carried out in the presence of Bz2O2 or AIBN as thermal initiator and hydrogen peroxide or benzophenone as photosensitizer. From the overall copolymerization product, the rubber-PMMA graft copolymer fraction was isolated from unreacted rubber and free PMMA fractions and composition characterization of the separated fractions was done by determination of rubber unsaturation. The efficiency of grafting under different conditions has been calculated and compared.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
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