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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 88-90 (Jan. 1992), p. 355-360 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 73 (1993), S. 2038-2038 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 75 (1994), S. 7514-7518 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Al-Co powder mixtures of several different compositions are mechanically alloyed by high-energy ball milling (HEBM) and then annealed. The structure analysis of x-ray diffraction and transmission electron microscopy revealed that the metastable phase obtained by HEBM decomposes to several stable phases during heating. The formed phases include decagonal quasicrystal (DQC), a new approximant of DQC, and several other known crystal phases that appear to depend on the composition of powder mixture. Convergent-beam electron-diffraction analysis has also been taken to determine the space group of the new phase. Finally, the structural relation between the known Al3Co and the new phase is also discussed in view of the crystal symmetry.
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 71 (1992), S. 2945-2949 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: In this work the AlCo intermetallic compound has been prepared by high-energy ball milling of Co and Al powder mixtures with the composition of Co-50 at.% Al, Co-71.4 at.% Al, Co-76.5 at.% Al, and Co-81.8 at.% Al, respectively. X-ray diffraction and transmission electron microscopy analysis of powders milled for different times proved that the AlCo phase formed directly during milling of the powder mixture of the former three compositions. In the Co-81.8 at.% Al powder mixture the amorphous phase was first formed and then crystallized to the AlCo phase. The result of energy dispersion x ray showed that the composition of AlCo phase formed during milling of the above four compositions is in agreement with that of the powder mixture, although their crystal structure is that of the AlCo intermetallic compound. The results indicate that the solubility range of intermetallic compound during mechanical alloying processes can be greatly enhanced by high-energy ball milling. The enhancement of solubility is discussed based on the structural features of nanocrystals.
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  • 5
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 14 (1993), S. 1221-1227 
    ISSN: 1572-9567
    Keywords: Burnett apparatus ; HFC-32 ; refrigerants ; vapor pressure
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A slightly modified Burnett apparatus has been used to measure 32 vapor-pressure data for HFC-32 in the temperature range from 273.39 to 347.29 K. The uncertainties of temperature and pressure are estimated to be within ±10 mK and ±500 Pa, respectively. The purity of the sample used in this work is 99.95%. On the basis of our data and of data from the literature, a vapor-pressure equation for HFC-32 is also proposed.
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  • 6
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 15 (1994), S. 941-948 
    ISSN: 1572-9567
    Keywords: capillary rise ; HFC-125 ; refrigerant ; surface tension
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A set of accurate surface-tension data for HFC-125 has been obtained experimentally with both an absolute capillary rise technique and a differential capillary rise technique in the temperature range of 233.15–333.15 K. The purity of the experimental HFC-125 sample is 99.98 wt%. The two sets of experimental results with an absolute capillary rise method agree well with each other and, also, with the experimental results with a differential capillary rise method. The absolute deviations of experimental results with these two methods are within 0.01 mN · m−1. The relative deviation are within 0.2%. A van der Waals surface-tension correlation is also proposed.
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  • 7
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 14 (1993), S. 1039-1050 
    ISSN: 1572-9567
    Keywords: acoustic interferometer ; 1,1,1,2 tetraflouroethane ; R134a ; sound velocity ; specific heat
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A cylindrical, variable-path acoustic interferometer operating at 156.252kHz is developed for determining ideal-gas specific heats. Results of validation measurements with argon are very satisfactory, with the maximum deviation of the speed of sound equal to 3×10−4. The sound velocity of gaseous R134a has been measured at low temperatures and low pressures. The specific heat was then calculated from the results. The experimental results corrected for various dispersions for the sound velocity of gaseous R134a match well with an earlier publication, with a room mean square deviation of 2.56×10−4. A new relation for the ideal-gas specific heat as a function of temperature for R134a is obtained.
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  • 8
    Electronic Resource
    Electronic Resource
    Springer
    International journal of thermophysics 14 (1993), S. 1221-1227 
    ISSN: 1572-9567
    Keywords: Burnett apparatus ; HFC-32 ; refrigerants ; vapor pressure
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract A slightly modified Burnett apparatus has been used to measure 32 vapor-pressure data for HFC-32 in the temperature range from 273.39 to 347.29 K. The uncertainties of temperature and pressure are estimated to be within ±10 mK and ±500 Pa, respectively. The purity of the sample used in this work is 99.95%. On the basis of our data and of data from the literature, a vapor-pressure equation for HFC-32 is also proposed.
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  • 9
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 26 (1991), S. 5527-5533 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Microstructures of martensite in a Cu-26.4Zn-4.8Al shape memory alloy after deformation and thermomechanical cycles are reported. By detailed transmission electron microscopy investigation, it is clearly established that the microstructure induced by deformation is different from that induced by thermomechanical cycles, and the effects on the thermoelastic martensite transformation are also not the same at all. The microstructure of martensite induced by deformation is mainly deformation twins when the deformation exceeds the range of recoverable strain of the shape memory alloy. The main microstructure characteristic of martensite which has undergone thermomechanical cycles is regularly distributed dislocations, which are mainly aligned but sometimes tangled. Micro-twins similar to those found in deformed martensite and crossed bands also exist inside the martensite of samples after thermomechanical cycles, but the amounts are too small to be regarded as important microstructure features.
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  • 10
    Electronic Resource
    Electronic Resource
    Springer
    Journal of materials science 25 (1990), S. 2047-2052 
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract In the present paper, the crystallography of isothermal transformation and decomposition ofβ, phase have been studied by means of transmission electron microscopy and diffraction in the CuZnAl shape memory alloy. It has been proved that the bainite formed inβ 1, matrix when the samples were transformed isothermally at moderate temperature. The crystallography of the isothermal bainitic transformation is identical to that of martensite in the same system. When the specimens were aged at moderate temperatures for longer time, the bainite and matrix decomposed to equilibrium phases. The decomposition process can be summarized as follows: $$\begin{gathered} bainite (9R) \to 9R + \alpha \left( {fcc} \right) \to \alpha + \beta \left( {bcc} \right) \hfill \\ matrix (B2) \to 2H + B2 \to \beta \left( {bcc} \right) \hfill \\ \end{gathered} $$ There are definite orientation relationships among these phases during the decomposition process and they are shown below: $$\begin{gathered} \left( {111} \right)_\alpha \parallel \left( {001} \right)_B ,\left[ {0\bar 11} \right]_\alpha \parallel \left[ {\bar 110} \right]_B \hfill \\ \left( {111} \right)_\alpha 5^ \circ away from \left( {110} \right)_\beta ,\left[ {0\bar 11} \right]_\alpha \parallel \left[ {1\bar 1\bar 1} \right]_\beta \hfill \\ \left( {110} \right)_M \parallel \left( {001} \right)_{2H} ,\left[ {001} \right]_M \parallel \left[ {010} \right]_{2H} \hfill \\ \end{gathered} $$ Thus, the crystallography of isothermal transformation and decomposition ofβ 1 phase and the sequence of transitions have been revealed.
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