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Crystal structure of phenyl bis(O-isopropylxanthato s,s′)arsenic(III) (1992)

Karra, R. ; Singh, Y. P. ; Bohra, R. ; [et al.]

Springer

Journal of chemical crystallography 22 (1992), S. 721-724

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ISSN: 1572-8854

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract The crystal structure of the title compound PhAs(S2COPri)2 has been determined by single crystal X-ray diffraction and refined by full matrix least squares analysis with anisotropic temperature factors. The crystal is monoclinic, space groupP21/c,a=8.889(6),b=16.174(19),c=13.506(14) Å,β=102.02(7)°,V=1899.2 Å3,Z=4,D c=1.478 g cm−3, monochromated Mo-Kα radiation, λ=0.71069 Å,μ=22.07 cm−1. The geometry around the arsenic atom is square pyramidal. Each ligand is bonded to an arsenic atom through two unequal As-S bonds measuring 2.298 and 3.041 Å. The apical position is occupied by a phenyl group and a lone pair of electrons is presenttrans to the phenyl group.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01160992

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