ISSN:
0749-1581
Keywords:
NMR
;
1H NMR
;
13C NMR
;
1D TOCSY
;
2D HMQC TOCSY
;
steroids
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The complete assignments of 1H and 13C data for two steroid epoxides, 3β-acetoxy-5,6β-epoxyandrostan-17-one and 3β-acetoxy-5,6β-epoxycholestane, based on DEPT, 1H—1H DQF COSY, HMQC, 1D TOCSY and 2D HMQC TOCSY sequences are described. Especially the 1D TOCSY and 2D HMQC TOCSY techniques were essential to the structure elucidation of theses steroids.
Additional Material:
2 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260330312
Permalink