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  • 1
    Electronic Resource
    Electronic Resource
    Zur Struktur des Chromtetrafluorids (1995)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 621 (1995), S. 1969-1972 
    Details
    ISSN: 0044-2313
    Keywords: Chromium tetrafluoride ; single crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Structure of Chromium TetrafluorideBy direct fluorination of elemental chromium with a HF/F2-mixture under solvothermal conditions CrF4 has been obtained for the first time in form of single crystal suitable for x-ray investigations. The violet till amethyst coloured CrF4 crystallizes tetragonal, space group P42/mnm-D4h14 (Nr. 136), a = 829.6(1) pm, c = 373.7(1) pm, Z = 4 and is closely related to the NbOCl3-type of structure [1].
    Notes: Durch Druckfluorierung von elementarem Chrom mit einem HF/F2-Gemisch unter Solvothermalbedingungen gelang es erstmals, CrF4 in Form zur Strukturbestimmung geeigneter Einkristalle darzustellen. Das violette bis amethystfarbene, häufig nadelförmige Chromtetrafluorid kristallisiert tetragonal in der Raumgruppe P42/mnm-D4h14 (Nr. 136) mit a = 829,6(1) pm, c = 373,7(1) pm, Z = 4 und ist vom Aufbau her dem NbOCl3-Typ eng verwandt [1].
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19956211123
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  • 2
    Electronic Resource
    Electronic Resource
    Zur Kristallstruktur von O2+MF6- (M = Sb, Ru, Pt, Au) (1996)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 622 (1996), S. 1076-1082 
    Details
    ISSN: 0044-2313
    Keywords: Dioxygenyl compounds ; single crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: On the Crystal Structure of O2+MF6- (M = Sb, Ru, Pt, Au)O2+MF6- (M = Sb, Ru, Pt, Au) were obtained again, but for the first time investigated by X-ray methods. Colourless O2+SbF6- and the rubyred compounds O2+RuF6- and O2+PtF6- crystallize isostructural in space group Ia3-Th7 (Nr. 206) with a = 1016(1) pm (Sb), a = 1002.6(9) pm (Ru) and a = 1003.6(9) pm (Pt), Z = 8. Yellow O2+AuF6- crystallizes trigonal-rhombohedric in space group R3-D326 (Nr. 148) with a = 775.9(3) pm, c = 711.7(4) pm, Z = 3.
    Notes: Erneut dargestellt, aber erstmals anhand von Einkristallen röntgenographisch untersucht wurden die Fluoride O2+MF6- (M = Sb, Ru, Pt, Au). Farbloses O2+ und die rubinroten Verbindungen O2+RuF6- und O2+PtF6- kristallisieren isotyp in der Raumgruppe Ia3-Th7 (Nr. 206) mit a = 1016(1) pm (Sb), a = 1002,6(9) pm (Ru) und a = 1003,6(9) pm (Pt), Z = 8. Gelbes O2+AuF6- kristallisiert trigonal-rhomboedrisch in der Raumgruppe R3-D326 (Nr. 148) mit a = 775,9(3) pm, c = 711,7(4) pm, Z = 3.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19966220623
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  • 3
    Electronic Resource
    Electronic Resource
    CsTi8F33 - nach (O2)2Ti7F30 der letzte Zwischenschritt zur TiF4-Struktur? (1995)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 621 (1995), S. 1223-1226 
    Details
    ISSN: 0044-2313
    Keywords: Fluorotitanates(IV) ; preparation ; single crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: CsTi8F33 - the Last Step on the Way to TiF4CsTi8F33 has been prepared for the first time as a byproduct of the synthesis of TiF4. The colourless compound crystallizes trigonal in the spacegroup P31c-C3v4 (No. 159) with a = 862 pm, c = 1 902 pm and Z = 2.
    Notes: CsTi8F33 wurde erstmals in Form farbloser, transparenter Einkristalle als Nebenprodukt bei Versuchen zur Darstellung von TiF4-Einkristallen [1] erhalten. Es kristallisiert trigonal in der nicht zentrosymmetrischen Raumgruppe P31c-C3v4 (Nr. 159) mit a = 862 pm, c = 1 902 pm und Z = 2.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19956210719
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  • 4
    Electronic Resource
    Electronic Resource
    InBF4, das erste komplexe Fluorid mit Indium(I) (1997)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 623 (1997), S. 579-582 
    Details
    ISSN: 0044-2313
    Keywords: Indium(I) tetrafluoroborate ; single crystal structure ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: InBF4, the First Complex Fluoride with Indium(I)InBF4 has been obtained for the first time by reaction of indium metal with anhydrous HF and BF3 in form of colourless, transparent single crystals. It crystallizes orthorhombic, space group Pnma - D2h16 (Nr. 62) with a = 919.1(2), b = 577.1(1) and c = 737.0(2) pm. Z = 4 and it is isotypic to KBF4 respectively to baryt-typ.
    Notes: InBF4 wurde erstmals durch Umsetzung von metallischem Indium mit BF3 und wasserfreier HF in Form farbloser, transparenter Einkristalle erhalten. Es kristallisiert orthorhombisch, R. G. Pnma - D2h16 (Nr. 62) mit a = 919,1(2), b = 577,1(1) und c = 737,0(2) pm, Z = 4 und ist isotyp zu KBF4 bzw. damit dem Baryt-Typ.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19976230190
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