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  • Polymer and Materials Science  (4)
  • Inorganic Chemistry
  • 1995-1999  (4)
  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 29 (1998), S. 254-257 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Measurement of three-dimensional residual stresses at rolled bars with high hardnessBars out of 56 Ni Cr Mo V 7, a diameter of 63 mm and a length of 100 mm were rolled with a force of 12 kN and 27 kN. The hardness of the bars was 2150 N/mm2. In 8 different direction along the surface the residual stresses were determined with the help of x-ray diffraction. This was done several times after electrolytic reduction of the material at the measuring zone to get a stress profile in dependence of the depth. Afterwards in two dimensions along the surface and perpendicular to the surface the residual stresses inclusive the shear stresses were determined. High compressive residual stresses were along the surface, but therefore tensile residual stresses were perpendicular to the surface at a zone of around 1.5 mm depth. A comparison of the residual stresses with stresses induced by shot peening is done.
    Notes: Bei der Bestimmung der 3dimensionalen Eigenspannungszustände zeigt sich, daß die einzelnen Eigenspannungsverläufe miteinander korrespondieren. Die Druckeigenspannungsbereich reicht beim Festwalzen bis in eine Tiefe von 2 mm, wobei sich ein Druckeigenspannungsplateau im Bereich ab 0,5 mm Tiefe für mehre Zehntel Millimeter ausbildet. Bei F=27 kN sind die Effekte entsprechend ausgeprägter. Im Vergleich zum Festwalzen ist beim Kugelstrahlen die Druckeigenspannung im Bereich bis 0.5 mm Tiefe zu finden.
    Additional Material: 9 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 27 (1996), S. 345-349 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Ultrafeine ZrO2 - Pulver durch Laserverdampfung: Herstellung und EigenschaftenUltrafeine oxidische Pulver werden durch Co2-Laserverdampfung aus grobem ZrO2-Pulver oder kompakten ZrO2-Stangen hergestellt.Die 10.6 μm-Strahlung im Leistungsbereich von 1 bis 4 kW wird durch einen quergeströmten CO2-Laser erzeugt, der in cw-und Pw-Betrieb arbeitet.Die Verdampfungsrate ist abhängig von der relativen Lage der Fokalebene zur Oberfläche des ZrO2-Pulvers, der Laserintensität und der eingekoppelten Energie.Bei einer Laserintensität von 4.2 · 105 Wcm-2 erreicht man eine optimale Verdampfungsrate von 130 g · h-1 (cw-Betrieb des Lasers).Das hergestellte Pulver besteht aus sphärischen Partikeln; deren Durchmesser variiert im Bereich von 5 bis 200 nm und kann durch die Verfahrensparameter beeinflußt werden. Die spezifische Oberfläche ist einstellbar von 10 bis 30 m2 · g-1.Das Pulver aus unstabilisiertem Zirkonium besitzt einen sehr hohen Anteil tetragonaler Phase. Im Fall von chemisch stabilisiertem Zirkonium kann sich die Zusammensetzung während des Verdampfungsprozesses und der Rekondensation ändern.
    Notes: Ultrafine oxide powders were produced by CO2 laser evaporation of coarse ZrO2 powder or compact stabilized ZrO2 materialThe 10.6μm radiation in the power range 1-4kW was generated by a transversal flow Co2 laser which can oscillate in cw and pw operationThe vaporization rate depends on the relative position of the focal plane to the surface of the ZrO2 powder, the laser intensity and the supplied energy input.At a laser intensity of 4.2 · 105 Wcm-2 the optimum vaporization rate is 130 g · h-1 (cw-operation of the laser).The produced powders consist of spherical particles; their diameters vary in the range from 5 to 200 nm can be controlled by the process conditions. The surface area (BET) is adjustable from 10 to 30 m2 · g-1.The powders of unstabilized zirconia show an unusual high content of the tetragonal phase. In case of chemically stabilized zirconia the composition can change during the process of evaporation and recondensation.
    Additional Material: 9 Ill.
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  • 3
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 27 (1996), S. 354-358 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Materialwissenschaft und Werkstofftechnik 28 (1997), S. 549-556 
    ISSN: 0933-5137
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Reduction of Residual Stresses at stress peened Torsion Bars under dynamic Load
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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