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  • Analytical Chemistry and Spectroscopy  (4)
  • Cyclodextrins
  • 2,8-dimethyl-1,7-dioxaspiro[5.5]undecane
  • 1995-1999  (4)
Collection
Keywords
Publisher
Years
Year
  • 1
    Electronic Resource
    Electronic Resource
    Separation of basic drugs by capillary electrophoresis using selectively modified cyclodextrins as chiral selectors (1995)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Microcolumn Separations 7 (1995), S. 355-363 
    Details
    ISSN: 1040-7685
    Keywords: basic drugs ; capillary electrophoresis ; cyclodextrin derivatives ; separation of enantiomers ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The influence of seven differently methylated β-cyclodextrin derivatives and of pure β-cyclodextrin (β-CD) on the enantiomeric resolution by capillary electrophoresis of six basic chiral pharmaceuticals is investigated. The methyl substitution pattern affects enantioselectivity much more than other experimental parameters. The purity of the used cyclodextrin derivatives is analyzed by successive hydrolysis, reduction, acetylation, and GC/MS of each CD derivative and by MALDI-TOF mass spectrometry. © 1995 John Wiley & Sons, Inc.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mcs.1220070408
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  • 2
    Electronic Resource
    Electronic Resource
    Enantiomeric composition of the chiral constituents of essential oils - part 3: Diterpene hydrocarbons (1997)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 20 (1997), S. 257-260 
    Details
    ISSN: 0935-6304
    Keywords: Enantioselective GC ; Diterpene Hydrocarbons ; Cyclodextrin derivatives ; Essential oils ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Enantiomeric diterpene hydrocarbons were isolated from different plants and identified by mass spectrometric and NMR investigations. All enantiomeric pairs could be resolved by capillary gas chromatography using either heptakis(2,6-di-O-methyl-3-O-pen-tyl)-β-cyclodextrin or heptakis(6-O-tert-butyldimethylsilyl-2,3-di-O-methyl)-β-cyclodextrin as chiral stationary phases.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240200503
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  • 3
    Electronic Resource
    Electronic Resource
    Chloro-bis-propyl Ethers in the Elbe River - Isomeric Distribution and Enantioselective Degradation (1998)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 21 (1998), S. 113-120 
    Details
    ISSN: 0935-6304
    Keywords: Enantioselective GC of chlorinated bis(propyl) ethers ; environmental analysis ; contamination of the Elbe River ; cyclodextrin derivatives ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: ---Cyclodextrin derivatives are evaluated as chiral stationary phases for the enantiomer separation of chlorinated bis(propyl) ethers (BPE). The enantiomeric composition of the 2,3,2′,3′- and 1,3,2′,3′-isomers of tetrachlorobis(propyl) ether in the Elbe River has been quantitatively determined by enantioselective gas chromatography and coupled gas chromatography/mass spectrometry in selected-ion-monitoring mode. Significant enantiomeric discriminations are observed in selected water samples, indicating that enantioselective bio-degradation mechanisms are at least partly responsible for the overall degradation processes.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Adulteration or natural variability? enantioselective gas chromatography in purity control of essential oils (1997)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 20 (1997), S. 55-61 
    Details
    ISSN: 0935-6304
    Keywords: Enantioselective gas chromatography ; Essential oils ; Authenticity control ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The potential of enantioselective capillary gas chromatography with modified cyclodextrins as chiral stationary phases for authenticity control is demonstrated for a selection of economically important essential oils. Adulteration can be easily detected in cases where enantiomerically pure constituents are present in natural oils. In cases of (naturally) varying enantiomeric compositions of chiral constituents, enantioselective gas chromatography may prove insufficient.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240200202
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