ISSN:
1573-4870
Keywords:
Lithium antimony oxide
;
chemical bath deposition
;
thermal decomposition
Source:
Springer Online Journal Archives 1860-2000
Topics:
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
Notes:
Abstract Well-crystallized LiSb(OH)6 powders with a hexagonal structure were prepared by chemical bath deposition. The thermal decomposition of as-prepared samples was examined. In order to obtain LiSb(OH)6 powders, it was essential to use tartaric acid as a stabilizing agent for antimony ion and to add LiOH above pH 9 into the precursor solution. The crystal structure of the samples obtained was of hexagonal phase. The increase in pH value and keeping temperature indicated that the shape of samples changed from granule particles to plate-like particles. The granule particles heated at 800°C consisted of orthorhombic LiSbO3. However, the plate-like particles resulted in the coexistence of both orthorhombic LiSbO3 and tetragonal Li3SbO4
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1023/A:1022677721231
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