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  • 1
    ISSN: 0022-4596
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Chemistry and Pharmacology
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Structures of Fluorides with Caesium. IV. The Crystal Structure of CsCrF4 - a Novel Tetra-fluorometallate Type with Chain StructureThe crystal structure of the hexagonal compound CsCrF4, crystallizing in space group P62m-D3h3, was determined: a =9.650(5), c = 3.857(3) Å, z = 3, R = 0.023 for 220 symmetrically independent reflections hkl. CsCrF4 is a new type of chain structure, containing three chains of octahedra sharing trans corners along [001] and connected by cis corners to form a triple chain. The bridging angles are Cr—F—Cr = 177.9° and 149.3°, the corresponding distances Cr—F = 1.929 and 1.940 Å, resp., compared to 1.851 Å for the terminal ligands. The results are discussed and relations to other structures shown.
    Notes: Die Kristallstruktur der hexagonal in der Raumgruppe P62,-D3h3 krikristallisierenden Verbindung CsCrF4 wurde bestimmt: a = 9,650(5), c = 3,857(3) Å, V = 311,1 Å3, z = 3, R = 0,023 für 220 symmetrieunabhängige Reflexe hkl. CsCrF4 stellt eine neuen Typ von Kettenstruktur dar, in dem drei längs [001] über trans-Ecken verknüpfte Oktaederketten miteinander über cis-Ecken zu einem Dreierstrang verbunden sind. Die Brückenwinkel betragen Cr—F—Cr 177,9° bzw. 149,3°, die entsprechenden Abstände Cr—F = 1,929 bzw. 1,940 Ä, gegenüber 1,851 Å für die terminalen Liganden. Die Ergebnisse werden diskutiert und Beziehungen zu anderen Strukturen aufgezeigt.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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  • 3
    In:  Other Sources
    Publication Date: 2019-07-13
    Description: Pressure and speed of sound measurements are used to obtain averaged gas properties in a Ludwieg combustion tube in which the gas is burned just prior to use. Absorption of a laser beam in the exit flow is used to check the predicted temperature uniformity. The burning process and the heat transfer to the cold walls are modeled. Interferograms of Ludwieg tube boundary layers are utilized to develop a new semiempirical boundary layer expression referred to as the integral density thickness, which is then applied to a recently developed linearized analysis of the effects of this layer. Pressure-time histories are determined for a wide range of tube flow Mach number and aspect ratio. Viscous and nonviscous effects are considered. It is shown that although the influence of the integral density thickness on the flow can be large, a modified linear theory can be used to estimate the effects for arbitrary tube flow Mach number and values of the aspect ratio that include cases where the boundary layers have merged.
    Type: Modern developments in shock tube research; July 14-16, 1975; Kyoto; Japan
    Format: text
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