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  • 1
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Contributions to the Chemistry of Transition Metal Diolefin Complexes. IV. Synthesis of Cobalt Coordination Compounds of Butadiene-d6The synthesis and characterization of two cobalt complexes of butadiene-1, 3-d6 with the empirical formula CoC12D19 and CoC12D18H will be described. The results of the mass spectroscopy and the 1H-NMR studies lead to the proposed structure:.1(π-butadiene-1, 3-d6)(π-3-methyl-d3-heptadienyl-d10)cobalt.2(π-butadiene-1, 3-d6)(π-3-methyl-d2-heptadienyl-d10)cobalt. .The mechanism of synthesis of the named complexes will be reported.
    Notes: Die Darstellung und Charakterisierung von zwei Kobaltkomplexen des perdeuterierten Butadiens mit den Summenformeln CoC12D19 (1) bzw. CoC12D18H (2) wird beschrieben. Die Ergebnisse der Massenspektroskopie und der 1H-NMR-Studien führen zu folgenden Strukturvorschlägen:.1(π-Butadien-1, 3-d6)(π-3-methyl-d3-heptadienyl-d10)kobalt.2(π-Butadien-1, 3-d6)(π-3-methyl-d2-heptadienyl-d10)kobalt..Der Mechanismus zur Bildung der beiden π-Komplexe wird beschrieben.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
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