ISSN:
1013-9826
Source:
Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
Topics:
Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
Notes:
The nano-powder of Al2O3-SiO2-CaF2 bio-glass was prepared by the homo-precipitation method with some inorganic salts containing Al3+, Ca2+, Na+, F-, SiO32+, Cl- as starting-reagents. The composition and characteristics of the powders were studied with XRD, EDAX, TEM and DTA. The results indicate that the prepared powder belongs to amorphous compounds containing Al, Ca, Si, O andF atoms and the size of particle is in the range of 30 ~ 70 nm. Adding citric acid and the well-controlled desiccation process can slightly improve the dispersing effect of the powders; the mixture ratio of the reagents rarely affects the characteristic of powder. The crystal phase CaF2 was precipitated firstly from the amorphous structure when the temperature is above 600°C, with the temperature rising, Al2SiO5 and Al4.4Si1.2O9.5 etc. crystal phases were precipitated sequentially
Type of Medium:
Electronic Resource
URL:
http://www.tib-hannover.de/fulltexts/2011/0528/01/49/transtech_doi~10.4028%252Fwww.scientific.net%252FKEM.280-283.1643.pdf
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