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Thermogravimetric analysis for boiling points and vapour pressure (1996)

Goodrum, J. W. ; Siesel, E. M.

Springer

Journal of thermal analysis and calorimetry 46 (1996), S. 1251-1258

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ISSN: 1572-8943

Keywords: boiling points ; DSC ; TGA ; vapour pressure

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract A TGA instrument has been adapted for rapid measurement of boiling points and vapour pressure at temperatures from ambient up to 400°C and pressures from ambient down to 20 mm Hg. Samples were contained in sealed holders having a laser-drilled aperture. Several organic liquids in the 100 to 300 gMW range showed good agreement with reference vapour pressure data. Sample mass, heating rate, and use of inert diluents were important variables affecting accuracy of vapour pressure measurements.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF01979239

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