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  • 1
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    Silsesquioxane-derived ceramic fibres (1991)
    Springer
    Details
    Publication Date: 1991-01-01
    Print ISSN: 0022-2461
    Electronic ISSN: 1573-4803
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Published by Springer
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  • 2
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    Pyrolytic conversion of methyl- and vinylsilane polymers to Si-C ceramics (1995)
    Springer
    Details
    Publication Date: 1995-06-01
    Print ISSN: 0022-2461
    Electronic ISSN: 1573-4803
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Published by Springer
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  • 3
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    Characterization of the pyrolytic conversion of polysilsesquioxanes to silicon oxycarbides (1993)
    Springer
    Details
    Publication Date: 1993-12-01
    Print ISSN: 0022-2461
    Electronic ISSN: 1573-4803
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Published by Springer
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  • 4
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    Silsesquioxane-derived ceramic fibres (1991)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: Fibers formed from blends of silsesquioxane polymers were characterized to study the pyrolytic conversion of these precursors to ceramics. The morphology of fibers pyrolyzed to 1400 C revealed primarily amorphous glasses whose conversion to beta-SiC is a function of both blend composition and pyrolysis conditions. Formation of beta-SiC crystallites within the glassy phase is favored by higher than stoichiometric C/Si ratios, while carbothermal reduction of Si-O bonds to form SiC with loss of SiO and CO occurs at higher methyl/phenylpropyl silsesquioxane (lower C/Si) ratios. As the carbothermal reduction is assumed to be diffusion controlled, the fibers can serve as model systems to gain understanding of the silsesquioxane pyrolysis behavior, and therefore are useful in the development of polysilsesquioxane-derived ceramic matrices and coatings as well.
    Keywords: NONMETALLIC MATERIALS
    Type: Journal of Materials Science (ISSN 0022-2461); 26; 1247-125
    Format: text
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  • 5
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    Silsesquioxanes as precursors to ceramic composites (1987)
    In:  Other Sources
    Details
    Publication Date: 2011-08-19
    Description: Silsesquioxanes having the general structure RSiO(1.5), where R = methyl, propyl, or phenyl, melt flow at 70 to 100 C. Above 100 C, free OH groups condense. At 225 C further crosslinking occurs, and the materials form thermosets. Pyrolysis, with accompanying loss of volatiles, takes place at nominally 525 C. At higher temperatures, the R group serves as an internal carbon source for carbo-thermal reduction to SiC accompanied by the evolution of CO. By blending silsesquioxanes with varying R groups, both the melt rheology and composition of the fired ceramic can be controlled. Fibers can be spun from the melt which are stable in argon in 1400 C. The silsesquioxanes also were used as matrix precursors for Nicalon and alpha-SiC platelet reinforced composites.
    Keywords: COMPOSITE MATERIALS
    Type: Ceramic Engineering and Science Proceedings (ISSN 0196-6219); 8; 732-743
    Format: text
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  • 6
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    Ethynylated aromatics as high temperature matrix resins (1987)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: Difunctional and trifunctional arylacetylenes were used as monomers to form thermoset matrix resin composites. Composites can be hot-pressed at 180 C to react 80 percent of the acetylene groups. Crosslinking is completed by postcuring at 350 C. The postcured resins are thermally stable to nominally 460 C in air. As a result of their high crosslink density, the matrix exhibits brittle failure when uniaxial composites are tested in tension. Failure of both uniaixial tensile and flexural specimens occurs in shear at the fiber-matrix interface. Tensile fracture stresses for 0-deg composites fabricated with 60 v/o Celion 6K graphite fiber were 827 MPa. The strain to failure was 0.5 percent. Composites fabricated with 8 harness satin Celion cloth (Fiberite 1133) and tested in tension also failed in shear at tensile stresses of 413 MPa.
    Keywords: NONMETALLIC MATERIALS
    Type: SAMPE Journal (ISSN 0091-1062); 23; 49-53
    Format: text
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  • 7
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    Off-axis tensile properties and fracture in a unidirectional graphite/polyimide composite (Celion 6000/PMR 15) (1984)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Description: Tensile properties of unidirectional Celion 6000 graphite/PMR 15 polyimide composites prepared by hot molding and cold molding processes were measured at room temperature and 316 C, the upper use temperature of the polyimide resin, at both 45 and 90 deg to the fiber axis. The resulting fractures were characterized by scanning electron microscopy and materialographic techniques. Variation in tensile properties with processing history occurred in the elastic modulus and strain to failure for specimens loaded at 90 deg at 316 C, and in the fracture stress, and hence the in-plane shear stress, for those loaded at 45 deg at room temperature. Significant plastic deformation was observed in the 45 deg orientation at 316 C for material produced by both processing methods. In general, fracture occurred by both failure within the matrix and at the fiber-matrix interface; the degree of interfacial failure increased with temperature. Secondary cracking below the primary fracture surface was also observed.
    Keywords: COMPOSITE MATERIALS
    Type: Polymer Composites (ISSN 0272-8397); 5; 179-185
    Format: text
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  • 8
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    The effect of a coating on the thermo-oxidative stability of Celion 6000 graphite fiber/PMR 15 polyimide composites (1983)
    In:  Other Sources
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    Publication Date: 2011-08-18
    Description: The thermooxidative stability in air at 316 C of unidirectional, uncoated and aluminum-coated Celion 6000 graphite fiber/PMR 15 polyimide composites has been determined for exposure times up to nominally 2000 h. Comparison of the weight loss data and microstructural integrity reveals that a thin aluminum-foil coating can provide significant protection from oxidation. A quantitative description of the average depth of the reaction zone and the maximum length of cracks produced during oxidation as a function of time in uncoated Celion 6000/PMR 15 are given.
    Keywords: COMPOSITE MATERIALS
    Type: Composites Technology Review; 5; 109-114
    Format: text
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  • 9
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    Application of a gripping system to test a uniaxial graphite fiber reinforced composite /PMR 15/Celion 6000/ in tension at 316 C (1982)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Description: A gripping system has been developed to test uniaxial, 0 deg orientation PMR 15/Celion 6000 composites at elevated temperatures. The method involves compression of grit-blasted laminate between grit-blasted metal to give a non-slipping interface for load transfer. Tensile testing at both 316 C and room temperature indicated that deformation was elastic to fracture and that the variation in tensile properties for one laminate is the same as that for several panels. In addition, the tensile properties for uniaxial PMR 15/Celion 6000 are identical at 316 C and room temperature. For nominally 51 volume percent fiber, the elastic modulus is 119.6 GPa, the fracture stress is 1370 MPa, and the strain to fracture is about 1.15 percent. In addition, data are presented which indicate that the gripping system can be used for long term, elevated temperature testing of composite materials.
    Keywords: COMPOSITE MATERIALS
    Type: Polymer Composites; 3; Apr. 198
    Format: text
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  • 10
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    On determination of fibre fraction in continuous fibre composite materials (1982)
    In:  Other Sources
    Details
    Publication Date: 2011-08-18
    Description: It is pointed out that the fiber volume fraction is probably the most important parameter influencing the properties of fibrous composite materials. The present investigation is concerned with questions regarding the accurate determination of this parameter. It is found that an estimate of the fiber volume fraction based on determinations from several coupons taken from different regions of a laminate is not accurate. At present fiber volume fractions are not directly measured but rather are calculated from the fiber weight fraction and densities of the composite and fiber. Image analysis techniques can and should be applied to determine fiber volume fraction. However, several factors have to be considered in this connection. It is necessary to make many measurements of the local fiber area fractions, and the preparation of representative planar cross sections parallel to the fiber axis may be difficult.
    Keywords: COMPOSITE MATERIALS
    Type: Journal of Materials Science Letters; 1; June 198
    Format: text
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