ISSN:
0749-1581
Keywords:
Trichothecene mycotoxins
;
Apotrichothecene
;
10,13-Cyclotrichothecane
;
13C NMR
;
2D NMR
;
1H—13C
;
NOE difference spectra
;
Spin-echo J modulation
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
A general strategy, using well established techniques, is outlined for the assignment of signals in the 13C NMR spectra of the trichothecene mycotoxins and some related rearrangement products. Heteronuclear NOE difference spectra were employed to assign resonances from quaternary carbons. An example of the use of spin-echo J modulation is given.
Additional Material:
2 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260260608
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