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  • 1
    Electronic Resource
    Electronic Resource
    Trichlorphosphazophosphordichlorid, Cl3P=N—PCl2Professor Kurt Issleib zum 60. Geburtstage gewidmet (1979)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 458 (1979), S. 103-107 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Trichlorophospnazophosphorusdichloride, Cl3P = N—PCl2P2NCl7 reacts with 2-chloroacrylonitrile to give the title compound. With P(C6H5)3 the compound (C6H5)3P=N—PCl2 is formed, which can be converted into (C6H5)3P=N—P(O)Cl2 by chlorine and SO2. The compounds are characterized by their properties and especially by their 31P n.m.r. spectra.
    Notes: P2NCl7 reagiert mit 2-Chloracrylnitril unter Bildung der Titelverbindung. Aus dieser entsteht bei der Umsetzung mit P(C6H5)3, (C6H5)3 P=N—PCl2, das mit Chlor und SO2 in (C6H5)3P=N—P(O)Cl2 übergeführt werden kann. Die Verbindungen werden durch ihre Eigenschaften und besonders durch ihre 31P-NMR-Spektren charakterisiert.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19794580114
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  • 2
    Electronic Resource
    Electronic Resource
    Reaktionen des Trichlorphosphazophosphordichlorids, Cl3P=N—PCl2Professor Josef Goubeau zum 80. Geburtstage am 31. März 1981 gewidmet (1981)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 474 (1981), S. 105-112 
    Details
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Reactions of Trichlorophosphazophosphorusdichloride, Cl3P=N—PCl2P2NCl5 reacts with SbF3 to give P2NCl3F2 from which P2NCl4F is obtained by chlorination. Sulfur oxidizes P2NCl5 to yield SP2NCl5, SO2 to yield SP2NCl5 and OP2NCl5. Reaction product from P2NCl5 and H2S is SPCl2(NH2) besides PCl3. P2NCl5 reacts with (n-C4H9)3P to give (n-C4H9)3P=N—PCl2. All new compounds are characterized by their n.m.r. spectra and their chemical behaviour.
    Notes: P2NCl5 reagiert mit SbF3 zu P2NCl3F2, aus dem mit Chlor P2NCl4F erhalten wird. Schwefel oxidiert P2NCl5 zu SP2NCl5, SO2 zu SP2NCl5 und OP2NCl5. Reaktionsprodukt aus P2NCl5 und H2S ist SPCl2(NH2) neben PCl3. Mit (n-C4H9)3P reagiert P2NCl5 zu (n-C4H9)3P=N—PCl2. Alle neuen Verbindungen sind durch ihre NMR-Spektren und ihr chemisches Verhalten charakterisiert.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19814740311
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