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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 353-358 (Sept. 2007), p. 2092-2095 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: In order to contribute to the development of the joining technique of Cf/SiC, joining ofSiC ceramic to high strength graphite was investigated. This joining has been successfully realizedby reaction joining process using a preceramic polymer, polysiloxane, mixed with the activeadditive Al-Si powder as joining material. The weld strength is strongly affected by thetechnological parameters and the ingredient ratio (polysiloxane:Al-Si powder). The optimizedfactors have been obtained by orthogonal experiments, under which the achieved three-pointbending strength of the joints is 96.8% of the strength of the welding base material graphite. Themicrostructure and composition of the weld zone were analyzed by SEM, EDX and XRD. Theresults show that the joining material has transformed into a densified interlayer with the thicknessof about 15μm. Also, diffusion takes place in the interfacial area, which contributes to a soundinterfacial bonding. The interlayer is composed of SiC, Al2O3 and Si
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 368-372 (Feb. 2008), p. 1600-1602 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Joining of SiC ceramic to graphite is important from both technical and economical points ofview. High temperature brazing of recrystallized SiC ceramic to high strength graphite has been realizedusing Ni-51Cr (consisting of Ni + 51wt% Cr powders) powders as filler. The obtained maximumthree-point bending strength of joints is 32.3MPa, which is equal to 80.8% of the strength of the graphite.Microstructure and phase analysis reveals that interdiffusions and chemical reactions take place in theweld zone. A reaction layer and an interlayer form in the interfacial area. The reaction layer, of which thethickness is about 60-100μm, is contacted with the SiC ceramic. The interlayer with the thickness ofabout 200μm exists between the graphite and the reaction layer. The reaction layer is mainly composed ofNi2Si, while the interlayer is mainly composed of Cr23C6 and Ni2Si
    Type of Medium: Electronic Resource
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