Publication Date:
2022-05-04
Description:
We present new pressure calibration experiments demons trating that the piston cylinder apparatus is suit-able for experiments at pressure as low as 150 MPa. Two newly designed 25 mm furnace assembly have
been developed and calibrated using two differe nt calibration methods: the NaC l melting curve and the sol-ubility of H2 O in albitic and rhyolitic melts. The NaCl calibration experiments performed in the pressure range
150 –500 MPa yield the pressure correction that has to be applied to the nominal pressure in order to have the
equivalent (real) pressure on the sample. This correction varies as a function of the experime ntal pressure as
follows:
Pcorrection MPaðÞ¼ −0 :115xP nominal MPaðÞþ 78 : 23
The H 2O solubility experiments in albitic and rhyolitic melts con firm the corrections determined using the
NaCl calibration method. Moreover, because these experiments are performed at temperatures higher than
those used for NaCl calibration, they demonstrate that the pressure correction is not affected by temperature
in the range 800– 1000 °C. The accuracy of the pressure estimate associated wi th the calibration methods is ±
25 MPa.
The major advantage of using the new assemblies is that low pressure experiments, which require rapid
heating and quenching rates (e.g. volcanic and hydrothermal systems), can be performed with the same
ease and precision as standard high pressure experiments for which piston cylinder is routinel y used.
Description:
Sapienza — Università di
Roma, Istituto Nazionale di Geofisica e Vulcanologia, Depths of the
Earth Company, NSF EAR-0838563 to G. Moore, and Science Founda-tion Sweden to V.R. Troll.
References
Description:
Published
Description:
74-79
Description:
2.3. TTC - Laboratori di chimica e fisica delle rocce
Description:
JCR Journal
Description:
restricted
Keywords:
Piston cylinder
;
pressure calibration
;
low pressure
;
02. Cryosphere::02.04. Sea ice::02.04.04. Instruments and techniques
Repository Name:
Istituto Nazionale di Geofisica e Vulcanologia (INGV)
Type:
article
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