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  • 1
    ISSN: 1572-8854
    Keywords: 1-(4-Nitrobenzyl)pyridinium ; bis(maleonitriledithiolato)nickelate(II) complex ; X-ray structure
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract The structure of [NO2Py]2[Ni(mnt)2], as determined by x-ray single crystal analysis, consists of two 1-(4-nitrobenzyl)pyridinium cations and one [Ni(mnt)2]2− anion. The crystallographic data for the complex:monoclinic P21/n, a = 9.913(2) Å, b = 11.968(2) Å, c = 14.566(3) Å, β = 100.36(3)°, V = 1699.9(6) Å3, Z = 2. The [Ni(mnt)2]2− anion has a crystallographically imposed center of symmetry and exhibits a relatively planar structure. The cation, [NO2Py]+, adopts a conformation where both the aromatic rings are twisted to the C11-C10-N3 reference plane. The anions (A) and the cations (C) consist of alternating layers (i.e., of type ···C1A1C2A2C1A1C2···) along the c axis of the crystallographic unit cell.
    Type of Medium: Electronic Resource
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  • 2
    Publication Date: 2016-01-09
    Description: A new fault diagnosis method for rotating machinery based on adaptive statistic test filter (ASTF) and Diagnostic Bayesian Network (DBN) is presented in this paper. ASTF is proposed to obtain weak fault features under background noise, ASTF is based on statistic hypothesis testing in the frequency domain to evaluate similarity between reference signal (noise signal) and original signal, and remove the component of high similarity. The optimal level of significance α is obtained using particle swarm optimization (PSO). To evaluate the performance of the ASTF, evaluation factor Ipq is also defined. In addition, a simulation experiment is designed to verify the effectiveness and robustness of ASTF. A sensitive evaluation method using principal component analysis (PCA) is proposed to evaluate the sensitiveness of symptom parameters (SPs) for condition diagnosis. By this way, the good SPs that have high sensitiveness for condition diagnosis can be selected. A three-layer DBN is developed to identify condition of rotation machinery based on the Bayesian Belief Network (BBN) theory. Condition diagnosis experiment for rolling element bearings demonstrates the effectiveness of the proposed method.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 3
    Publication Date: 2015-10-10
    Description: The Shannon sampling principle requires substantial amounts of data to ensure the accuracy of on-line monitoring of roller bearing fault signals. Challenges are often encountered as a result of the cumbersome data monitoring, thus a novel method focused on compressed vibration signals for detecting roller bearing faults is developed in this study. Considering that harmonics often represent the fault characteristic frequencies in vibration signals, a compressive sensing frame of characteristic harmonics is proposed to detect bearing faults. A compressed vibration signal is first acquired from a sensing matrix with information preserved through a well-designed sampling strategy. A reconstruction process of the under-sampled vibration signal is then pursued as attempts are conducted to detect the characteristic harmonics from sparse measurements through a compressive matching pursuit strategy. In the proposed method bearing fault features depend on the existence of characteristic harmonics, as typically detected directly from compressed data far before reconstruction completion. The process of sampling and detection may then be performed simultaneously without complete recovery of the under-sampled signals. The effectiveness of the proposed method is validated by simulations and experiments.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 4
    Publication Date: 2016-06-17
    Description: In the condition monitoring of roller bearings, the measured signals are often compounded due to the unknown multi-vibration sources and complex transfer paths. Moreover, the sensors are limited in particular locations and numbers. Thus, this is a problem of underdetermined blind source separation for the vibration sources estimation, which makes it difficult to extract fault features exactly by ordinary methods in running tests. To improve the effectiveness of compound fault diagnosis in roller bearings, the present paper proposes a new method to solve the underdetermined problem and to extract fault features based on variational mode decomposition. In order to surmount the shortcomings of inadequate signals collected through limited sensors, a vibration signal is firstly decomposed into a number of band-limited intrinsic mode functions by variational mode decomposition. Then, the demodulated signal with the Hilbert transform of these multi-channel functions is used as the input matrix for independent component analysis. Finally, the compound faults are separated effectively by carrying out independent component analysis, which enables the fault features to be extracted more easily and identified more clearly. Experimental results validate the effectiveness of the proposed method in compound fault separation, and a comparison experiment shows that the proposed method has higher adaptability and practicability in separating strong noise signals than the commonly-used ensemble empirical mode decomposition method.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 5
    Publication Date: 2016-09-20
    Description: The traditional approaches for condition monitoring of roller bearings are almost always achieved under Shannon sampling theorem conditions, leading to a big-data problem. The compressed sensing (CS) theory provides a new solution to the big-data problem. However, the vibration signals are insufficiently sparse and it is difficult to achieve sparsity using the conventional techniques, which impedes the application of CS theory. Therefore, it is of great significance to promote the sparsity when applying the CS theory to fault diagnosis of roller bearings. To increase the sparsity of vibration signals, a sparsity-promoted method called the tunable Q-factor wavelet transform based on decomposing the analyzed signals into transient impact components and high oscillation components is utilized in this work. The former become sparser than the raw signals with noise eliminated, whereas the latter include noise. Thus, the decomposed transient impact components replace the original signals for analysis. The CS theory is applied to extract the fault features without complete reconstruction, which means that the reconstruction can be completed when the components with interested frequencies are detected and the fault diagnosis can be achieved during the reconstruction procedure. The application cases prove that the CS theory assisted by the tunable Q-factor wavelet transform can successfully extract the fault features from the compressed samples.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 6
    Publication Date: 2011-07-21
    Description: The sparse decomposition based on matching pursuit is an adaptive sparse expression method for signals. This paper proposes an idea concerning a composite dictionary multi-atom matching decomposition and reconstruction algorithm, and the introduction of threshold de-noising in the reconstruction algorithm. Based on the structural characteristics of gear fault signals, a composite dictionary combining the impulse time-frequency dictionary and the Fourier dictionary was constituted, and a genetic algorithm was applied to search for the best matching atom. The analysis results of gear fault simulation signals indicated the effectiveness of the hard threshold, and the impulse or harmonic characteristic components could be separately extracted. Meanwhile, the robustness of the composite dictionary multi-atom matching algorithm at different noise levels was investigated. Aiming at the effects of data lengths on the calculation efficiency of the algorithm, an improved segmented decomposition and reconstruction algorithm was proposed, and the calculation efficiency of the decomposition algorithm was significantly enhanced. In addition it is shown that the multi-atom matching algorithm was superior to the single-atom matching algorithm in both calculation efficiency and algorithm robustness. Finally, the above algorithm was applied to gear fault engineering signals, and achieved good results.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 7
    Publication Date: 2019
    Description: In order to separate and extract compound fault features of a vibration signal from a single channel, a novel signal separation method is proposed based on improved sparse non-negative matrix factorization (SNMF). In view of the traditional SNMF failure to perform well in the underdetermined blind source separation, a constraint reference vector is introduced in the SNMF algorithm, which can be generated by the pulse method. The square wave sequences are constructed as the constraint reference vector. The output separated signal is constrained by the vector, and the vector will update according to the feedback of the separated signal. The redundancy of the mixture signal will be reduced during the constantly updating of the vector. The time–frequency distribution is firstly applied to capture the local fault features of the vibration signal. Then the high dimension feature matrix of time–frequency distribution is factorized to select local fault features with the improved SNMF method. Meanwhile, the compound fault features can be separated and extracted automatically by using the sparse property of the improved SNMF method. Finally, envelope analysis is used to identify the feature of the output separated signal and realize compound faults diagnosis. The simulation and test results show that the proposed method can effectively solve the separation of compound faults for rotating machinery, which can reduce the dimension and improve the efficiency of algorithm. It is also confirmed that the feature extraction and separation capability of proposed method is superior to the traditional SNMF algorithm.
    Electronic ISSN: 1099-4300
    Topics: Chemistry and Pharmacology , Physics
    Published by MDPI
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  • 8
    Publication Date: 2012-03-30
    Description: A least square method based on data fitting is proposed to construct a new lifting wavelet, together with the nonlinear idea and redundant algorithm, the adaptive redundant lifting transform based on fitting is firstly stated in this paper. By variable combination selections of basis function, sample number and dimension of basis function, a total of nine wavelets with different characteristics are constructed, which are respectively adopted to perform redundant lifting wavelet transforms on low-frequency approximate signals at each layer. Then the normalized lP norms of the new node-signal obtained through decomposition are calculated to adaptively determine the optimal wavelet for the decomposed approximate signal. Next, the original signal is taken for subsection power spectrum analysis to choose the node-signal for single branch reconstruction and demodulation. Experiment signals and engineering signals are respectively used to verify the above method and the results show that bearing faults can be diagnosed more effectively by the method presented here than by both spectrum analysis and demodulation analysis. Meanwhile, compared with the symmetrical wavelets constructed with Lagrange interpolation algorithm, the asymmetrical wavelets constructed based on data fitting are more suitable in feature extraction of fault signal of roller bearings.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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  • 9
    Publication Date: 2019
    Description: Given the increase in energy consumption and pollution emissions, China has formulated a low-carbon economic development strategy. Small and medium-sized enterprises (SMEs) are mostly at the bottom of the industrial chain and face problems of high energy consumption and low output. The problems of survival and sustainable development of SMEs are serious under the background of low-carbon economy. SMEs play an important role in optimizing economic structure and social stability. Thus, studying the survival and sustainable development strategies of SMEs in China is necessary. This study adopts the method of market survey to perform the questionnaire design, sample selection, questionnaire issuance, and data analysis from three perspectives of policy, social, and internal environments of SMEs. This study summarizes seven factors, including financing and operation management, which restrict the survival and sustainable development of SMEs in China under the background of low-carbon economy. Moreover, this study proposes specific suggestions from internal and external environments.
    Electronic ISSN: 2071-1050
    Topics: Energy, Environment Protection, Nuclear Power Engineering
    Published by MDPI
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  • 10
    Publication Date: 2012-05-03
    Description: A least square method based on data fitting is proposed to construct a new lifting wavelet, together with the nonlinear idea and redundant algorithm, the adaptive redundant lifting transform based on fitting is firstly stated in this paper. By variable combination selections of basis function, sample number and dimension of basis function, a total of nine wavelets with different characteristics are constructed, which are respectively adopted to perform redundant lifting wavelet transforms on low-frequency approximate signals at each layer. Then the normalized lP norms of the new node-signal obtained through decomposition are calculated to adaptively determine the optimal wavelet for the decomposed approximate signal. Next, the original signal is taken for subsection power spectrum analysis to choose the node-signal for single branch reconstruction and demodulation. Experiment signals and engineering signals are respectively used to verify the above method and the results show that bearing faults can be diagnosed more effectively by the method presented here than by both spectrum analysis and demodulation analysis. Meanwhile, compared with the symmetrical wavelets constructed with Lagrange interpolation algorithm, the asymmetrical wavelets constructed based on data fitting are more suitable in feature extraction of fault signal of roller bearings.
    Electronic ISSN: 1424-8220
    Topics: Chemistry and Pharmacology , Electrical Engineering, Measurement and Control Technology
    Published by MDPI Publishing
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