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  • 1
    Online Resource
    Online Resource
    Vibrational (Infrared and Raman) Spectra of Minerals and Related Compounds (2020)
    Cham :Springer International Publishing :
    Details
    Keywords: Mineralogy. ; Spectrum analysis. ; Ceramic materials. ; Materials Analysis. ; Mineralogy. ; Spectroscopy. ; Ceramics. ; Characterization and Analytical Technique.
    Description / Table of Contents: Chapter 1.Some Examples of the Use of IR Spectroscopy in Mineralogical Studies -- Chapter 2.IR Spectra of Minerals and Related Compounds, and Reference Samples Data -- Chapter 3.Some Aspects of the Use of Raman Spectroscopy in Mineralogical Studies -- Chapter 4.Raman Spectra of Minerals.
    Abstract: The book presents new data on the IR spectra of minerals and on the Raman spectra of more than 2000 mineral species. It also includes examples of IR spectroscopy applications to investigate minerals, and discusses the most important potential applications of Raman spectroscopy in mineralogical research. The book serves as a reference resource and a methodological guide for mineralogists, petrologists and technologists working in the field of inorganic materials.
    Type of Medium: Online Resource
    Pages: X, 1376 p. 1004 illus., 9 illus. in color. , online resource.
    Edition: 1st ed. 2020.
    ISBN: 9783030268039
    Series Statement: Springer Mineralogy,
    URL: https://doi.org/10.1007/978-3-030-26803-9
    DOI: 10.1007/978-3-030-26803-9
    DDC: 549
    Language: English
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  • 2
    Monograph available for loan
    Monograph available for loan
    Infrared spectra of mineral species : Extended library ; [Vol. 1] (2014)
    Dordrecht : Springer Netherlands
    Details
    Call number: M 17.90938
    Description / Table of Contents: Over the last 30 years, Dr. Nikita V. Chukanov has collected IR spectra of about 2000 mineral species, including 247 holotype samples. In this book, he presents 3309 spectra of these minerals with detailed  description and analytical data for reference samples. In the course of this work, about 150 new mineral species have been discovered. This book presents spectra of each mineral together with a description and comments on standard samples used (occurrence, appearance, associated minerals, empirical formula etc.). Sections are organized according to different classes of compounds (silicates, phosphates, arsenates, oxides etc.)
    Type of Medium: Monograph available for loan
    Pages: IX, 1726 p. 3547 illus., 1 illus. in color
    Edition: Online edition Springer eBook Collection. Earth and Environmental Science
    ISBN: 9789400771284 , 9789400771277 (print)
    Series Statement: Springer Geochemistry / Mineralogy
    DOI: 10.1007/978-94-007-7128-4
    Parallel Title: Print version Infrared spectra of mineral species : Extended library
    Language: English
    Note: The Application of IR Spectroscopy to the Investigation of MineralsThe Discrete Approach -- The Full-Profile Analysis -- Polymerization of coordination polyhedra and structure topology -- Hydrogen-bearing groups and hydrogen bonding -- Solid-solution series -- Force parameters of cations in silicates -- IR spectra of minerals and reference samples data -- Borates, including sulfato-borates and arsenato-borates -- Carbides and carbonates -- Organic compounds and salts of organic acids -- Ammino-complexes, nitrates and sulfato-nitrates -- Oxides and hydroxides -- Fluorides -- Silicates -- Phosphates -- Sulfates, carbonato-sulfates, phosphato-sulfates and sulfides -- Chlorides -- Vanadates and vanadium oxides -- Chromates -- Arsenates, arsenites and sulfato-arsenates -- Selenites, molybdates, tellurites, tellurates, iodites, wolframates and wolfram oxides..
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  • 3
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    New Data on the Isomorphism in Eudialyte-Group Minerals. 1. Crystal Chemistry of Eudialyte-Group Members with Na Incorporated into the Framework as a Marker of Hyperagpaitic Conditions (2020)
    Molecular Diversity Preservation International
    Details
    Publication Date: 2020-06-29
    Description: A review of the crystal chemistry of Fe-deficient eudialyte-group minerals is given. Specific features of cation distribution over key sites in the crystal structure, including partial substitution of Fe2+ with Na, Mn and Zr at the M2 site are discussed. It is concluded that Na-dominant (at the M2 site) eudialyte-group members (M2Na-EGMs) are markers of specific kinds of specific peralkaline (hyperagpaitic) igneous rocks and pegmatites. New data are obtained on the chemical composition, IR spectra and crystal chemistry for two samples of M2Na-EGMs with disordered M1 cations, which are a potentially new mineral species with the simplified formula (Na,H2O)15Ca6Zr3[Na2(Fe,Zr)][Si26O72](OH)2Cl·nH2O.
    Electronic ISSN: 2075-163X
    Topics: Geosciences
    Published by Molecular Diversity Preservation International
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  • 4
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    KOTTENHEIMITE, Ca3Si(OH)6(SO4)2·12H2O, A NEW MEMBER OF THE ETTRINGITE GROUP FROM THE EIFEL AREA, GERMANY (2012)
    Mineralogical Association of Canada
    Details
    Publication Date: 2012-02-01
    Description: The new ettringite-group mineral kottenheimite was found at Bellerberg, near Kottenheim, Eastern Eifel area, Rhineland- Palatinate (Rheinland-Pfalz), Germany, and named for the type locality. Associated minerals are wollastonite, clinochlore, ellestadite, melilite, cuspidine, and earlier formed sanidine, clinopyroxene, and magnetite. Kottenheimite forms white radiated and random aggregates of hair-like subparallel clusters of minute crystals. The Mohs’ hardness is 2–2.5; Dmeas = 1.92(2) g/cm3, Dcalc = 1.926 g/cm3. The new mineral is uniaxial (−), ω = 1.490(2), ɛ = 1.477(2). The IR spectrum of kottenheimite is in accordance with the chemical composition and contains absorption bands in the range 3300–3700 cm−1 (O–H-stretching vibrations), at 1650 and 1683 cm−1 (bending vibrations of H2O molecules), 1158, 1086, and 987 cm−1 (showing the presence of distorted SO42− groups), 752 and 725 cm−1 (corresponding to Si–O stretching vibrations of Si(OH)6 octahedra). The chemical composition is (electron microprobe, mean of 6 analyses, wt.%; H2O and CO2 determined by gas chromatography): CaO 26.04, MgO 0.20, FeO 0.19, Al2O3 0.25, SiO2 8.95, SO3 24.26, CO2 0.58, H2O 41.30; total 101.77. The empirical formula calculated on the basis of 26 anions is Ca3.015Mg0.03Fe0.02Al0.03Si0.97(OH)5.94(SO4)1.97(CO3)0.09·11.91H2O. The simplified formula is Ca3Si(OH)6(SO4)2·12H2O. The crystal structure was refined by the Rietveld method (Rp = 0.0487, Rwp = 0.0623, RB = 0.087) based on the structural model of carraraite, Ca3Ge(SO4,CO3)2(OH)6·12H2O. The new mineral is hexagonal, space group P63/m, a = 11.1548(3), c = 10.5702(3) Å, V = 1139.04(5) Å3, and Z = 2. The strongest lines of the powder diffraction pattern [d in Å (I) (hkl)] are: 9.72 (100) (100), 5.590 (60) (110), 4.645 (26) (102), 3.840 (54) (112), 2.751 (34) (302), 2.536 (27) (213), 2.185 (30) (223). The channels in the crystal structure of kottenheimite are only filled by sulfate anions and water molecules. Type material is deposited in the collections of the Fersman Mineralogical Museum of the Russian Academy of Sciences, Moscow, Russia, registration number 4102/1.
    Print ISSN: 0008-4476
    Topics: Geosciences
    Published by Mineralogical Association of Canada
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  • 5
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    Windhoekite, Ca2Fe3+3-x(Si8O20)(OH)4·10H2O, a new palygorskite-group mineral from the Aris phonolite, Namibia (2012)
    Schweizerbart
    Details
    Publication Date: 2012-01-01
    Description: The new mineral windhoekite was discovered in a specimen from the Ariskop Quarry, near Windhoek, Namibia. Associated minerals are fluorapophyllite, aegirine, microcline, arisite-(Ce), arisite-(La). Windhoekite is yellow-brown, translucent; streak is beige. It forms isolated long-prismatic crystals up to 0.15 × 4 mm and their radial aggregates in cavities in phonolite. Dcalc is 2.630 g/cm3, Dmeas is 2.62 (2) g/cm3. The new mineral is biaxial (-), a = 1.610(3), ß = 1.662(3), ? = 1.671(3), 2V (meas.) = 50(10)°, 2V (calc.) = 44°. Dispersion is not observed, pleochroism is strong (Y ˜ Z 〉X, brown to dark brown), orientation: X ˜ a; Z = c. The IR spectrum is given. The chemical composition is (electron microprobe, mean of 5 analyses, wt%): CaO 9.24, MnO 0.85, Fe2O3 23.14, Al2O3 0.41, SiO2 46.32, H2O (by gas chromatography) 21.0; total 100.96. The empirical formula based on 34 O atoms is: (Ca1.68Mn0.12)Fe3+2.96(Si7.87Al0.08O20)(OH)4·10H1.98O. The simplified formula is: Ca2Fe3+3-x[(Si,Al)8O20](OH)4·10H2O. The crystal structure was solved using single-crystal diffraction data. Windhoekite is monoclinic, space group C2/m, a = 14.319(5), b = 17.825(4), c = 5.242(1) Å, ß = 103.5(2)°, V = 1301.0(6) Å3, Z = 2. Ca and Fe3+ occupy two large octahedra and two smaller octahedra, respectively. The strongest lines of the powder diffraction pattern [d, Å (I, %) (hkl)] are: 11.04 (100) (110), 4.432 (10) (021), 4.133 (6) (22-1), 3.754 (4) (240), 3.486 (11) (400), 2.636 (8) (35-1), 2.551 (4) (002), 2.505 (6) (26-1). Type material is deposited in the collections of the Fersman Mineralogical Museum of the Russian Academy of Sciences, Moscow, Russia, under registration number 4018/1.
    Print ISSN: 0935-1221
    Electronic ISSN: 1617-4011
    Topics: Geosciences
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  • 6
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    Lileyite, Ba2(Na,Fe,Ca)3MgTi2(Si2O7)2O2F2, a new lamprophyllite-group mineral from the Eifel volcanic area, Germany (2012)
    Schweizerbart
    Details
    Publication Date: 2012-01-01
    Description: The new Mg- and F-dominant lamprophyllite-group mineral lileyite (IMA 2011-021) was found at the Löhley quarry, Üdersdorf, near Daun, Eifel Mountains, Rhineland-Palatinate (Rheinland-Pfalz), Germany, and named for the old name of the type locality, Liley. Associated minerals are nepheline, leucite, augite, magnetite, fluorapatite, perovskite, götzenite. Lileyite is brown, translucent; streak is white. It forms platy crystals up to 0.1 × 0.3 × 0.5 mm in size and their clusters up to 1 mm across on the walls of cavities in an alkaline basalt. Lileyite is brittle, with Mohs hardness of 3–4 and perfect cleavage on (001). Dcalc is 3.776 g/cm3. The new mineral is biaxial (+), a = 1.718(5), ß = 1.735(5), ? = 1.755(5), 2V (meas.) = 75(15)°, 2V (calc.) = 86°. The IR spectrum is given. The chemical composition is (EDS-mode electron microprobe, mean of 5 analyses, wt%): SiO2 28.05, BaO 26.39, TiO2 18.53, Na2O 6.75, MgO 4.58, FeO 4.48, CaO 2.30, SrO 2.23, MnO 1.44, K2O 1.41, Nb2O5 0.95, F 3.88, –O=F2 -1.63; total 99.36. The empirical formula based on 18 anions is: Ba1.50Sr0.19K0.26Na1.89Ca0.36Mn0.18Mg0.99Fe0.54Ti2.01Nb0.06Si4.06O16.23F1.77. The simplified formula is: Ba2(Na,Fe,Ca)3MgTi2(Si2O7)2O2F2. The crystal structure was solved using single-crystal X-ray diffraction data (R = 0.024). Lileyite is monoclinic, space group C2/m, a = 19.905(1), b = 7.098(1), c = 5.405(1) Å, ß = 96.349(5)°, V = 758.93(6) Å3, Z = 2. The strongest lines of the powder diffraction pattern [d, Å (I, %) (hkl)] are: 3.749 (45) (31–1), 3.464 (76) (510, 311, 401), 3.045 (37) (51–1), 2.792 (100) (221, 511), 2.672 (54) (002, 601, 20-2), 2.624 (43) (710, 42–1). Type material is deposited in the collections of the Fersman Mineralogical Museum of the Russian Academy of Sciences, Moscow, Russia, registration number 4106/1.
    Print ISSN: 0935-1221
    Electronic ISSN: 1617-4011
    Topics: Geosciences
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  • 7
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    Langbanshyttanite, a new low-temperature arsenate mineral with a novel structure from Langban, Sweden (2011)
    Schweizerbart
    Details
    Publication Date: 2011-08-01
    Description: The new mineral langbanshyttanite was discovered in a specimen from the Langban mine (59.86{degrees}N, 14.27{degrees}E), Filipstad district, Varmland County, Bergslagen ore province, Sweden. Associated minerals are calcite, Mn-bearing phlogopite, spinels of the jacobsite-magnetite series, antigorite and trigonite. The mineral is named after the old name of the mine, smelter and mining village: Langbanshyttan. Langbanshyttanite is transparent, colourless. It occurs in late-stage fractures or corroded pockets, forming soft, radial and random aggregates (up to 1 mm) of acicular crystals up to 5 x 20 x 400 {micro}m. Dcalc is 3.951 g/cm3. The new mineral is biaxial (+), {alpha} = 1.700(5), {beta} = 1.741(5), {gamma} = 1.792(5), 2V (meas.) {approx} 90{degrees}, 2V (calc.) = 86{degrees}. Dispersion is strong, r 〈 v. The IR spectrum is given. The chemical composition is (electron microprobe, mean of five analyses, wt%): PbO 44.71, MgO 3.79, MnO 13.34, FeO 1.89, P2O5 0.65, As2O5 22.90, H2O (determined by gas chromatographic analysis of the products of ignition at 1200 {degrees}C) 14.4; total 101.68. The empirical formula based on 18 O atoms is: Pb1.97Mn1.85Mg0.93Fe0.26(AsO4)1.96(PO4)0.09(OH)3.87{middle dot}5.93H2O. The simplified formula is: Pb2Mn2Mg(AsO4)2(OH)4{middle dot}6H2O. Single-crystal diffraction data obtained using synchrotron radiation indicate that langbanshyttanite is triclinic, P[IMG]f1.gif" ALT="Formula" BORDER="0"〉, a = 5.0528(10), b = 5.7671(6), c = 14.617(3) A, {alpha} = 85.656(14), {beta} = 82.029(17), {gamma} = 88.728(13){degrees}, V = 420.6(2) A3, Z = 1, and is a representative of a new structure type. In the structure, edge-sharing MnO2(OH)4 octahedra form zig-zag columns that are linked by isolated AsO4 tetrahedra. Pb cations having six-fold coordination are located between the AsO4 tetrahedra. Isolated Mg(H2O)6 octahedra are located in the inter-block space. The strongest lines of the powder diffraction pattern [d, A (I, %) (hkl)] are: 14.48 (100) (001), 7.21 (43) (002), 4.969 (34) (100, 101), 4.798 (28) (003), 3.571 (54) (112, 1-1-1, 01-3, 11-1), 2.857 (45) (020, 021, 114), 2.800 (34) (11-3). Parts of the holotype specimen are deposited in the Fersman Mineralogical Museum of Russian Academy of Sciences, Moscow, Russia, with the registration number 4032/1 and in the collections of the Swedish Museum of Natural History, Stockholm, Sweden, under catalogue number NRM 20100076.
    Print ISSN: 0935-1221
    Electronic ISSN: 1617-4011
    Topics: Geosciences
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  • 8
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    The new mineral novograblenovite, (NH4,K)MgCl3·6H2O from the Tolbachik volcano, Kamchatka, Russia: mineral description and crystal structure (2018)
    Mineralogical Society of Great Britain and Ireland
    Details
    Publication Date: 2018
    Description: 〈div data-abstract-type="normal"〉〈p〉The new mineral novograblenovite, (NH〈span〉4〈/span〉,K)MgCl〈span〉3〈/span〉·6H〈span〉2〈/span〉O, was found on basaltic lava from the 2012–2013 Tolbachik fissure eruption at the Plosky Tolbachik volcano, Kamchatka Peninsula, Russia. It occurs as prismatic, needle-like transparent crystals together with gypsum and halite. Novograblenovite was formed due to the exposure of the host rocks to eruptive gas exhalations enriched in HCl and NH〈span〉3〈/span〉. Basalt was the source of potassium and magnesium for the mineral formation. Novograblenovite crystallises in the monoclinic space group 〈span〉C〈/span〉2/〈span〉c〈/span〉, with unit-cell parameters 〈span〉a〈/span〉 = 9.2734(3) Å, 〈span〉b〈/span〉 = 9.5176(3) Å, 〈span〉c〈/span〉 = 13.2439(4) Å, β = 90.187(2)°, 〈span〉V〈/span〉 = 1168.91(2) Å〈span〉3〈/span〉 and 〈span〉Z〈/span〉 = 4. The five strongest reflections in the powder X-ray diffraction pattern [〈span〉d〈/span〉〈span〉obs〈/span〉, Å (〈span〉I〈/span〉, %) (〈span〉h k l〈/span〉)] are: 3.330 (100) (2 2 0), 2.976 (45) (〈span〉〈span〉〈img data-mimesubtype="gif" data-type="simple" src="http://static.cambridge.org/resource/id/urn:cambridge.org:id:binary:20190522072108342-0385:S0026461X18000889:S0026461X18000889_inline1.gif"〉 〈span data-mathjax-type="texmath"〉 〈/span〉 〈/span〉〈/span〉), 2.353 (29) (〈span〉〈span〉〈img data-mimesubtype="gif" data-type="simple" src="http://static.cambridge.org/resource/id/urn:cambridge.org:id:binary:20190522072108342-0385:S0026461X18000889:S0026461X18000889_inline2.gif"〉 〈span data-mathjax-type="texmath"〉 〈/span〉 〈/span〉〈/span〉), 3.825 (26) (2 0 2), 1.997 (25) (〈span〉〈span〉〈img data-mimesubtype="gif" data-type="simple" src="http://static.cambridge.org/resource/id/urn:cambridge.org:id:binary:20190522072108342-0385:S0026461X18000889:S0026461X18000889_inline3.gif"〉 〈span data-mathjax-type="texmath"〉 〈/span〉 〈/span〉〈/span〉 2). The density calculated from the empirical formula and the X-ray data is 1.504 g cm〈span〉–3〈/span〉. The mineral is biaxial (+) with α = 1.469(2), β = 1.479(2) and γ = 1.496(2) (λ = 589 nm); 2V〈span〉meas.〈/span〉 = 80(10)° and 2V〈span〉calc.〈/span〉 = 75.7°. The crystal structure (solved and refined using single-crystal X-ray diffraction data, 〈span〉R〈/span〉〈span〉1〈/span〉 = 0.0423) is based on the perovskite-like network of (NH〈span〉4〈/span〉,K)Cl〈span〉6〈/span〉-octahedra sharing chlorine vertices, and comprises [Mg(H〈span〉2〈/span〉O)〈span〉6〈/span〉]〈span〉2+〈/span〉 groups in framework channels. The positions of all independent H atoms were obtained by difference-Fourier techniques and refined isotropically. All oxygen, nitrogen and chlorine atoms are involved in the system of hydrogen bonding, acting as donors or acceptors. The formula resulting from the structure refinement is [(NH〈span〉4〈/span〉)〈span〉0.7〈/span〉K〈span〉0.3〈/span〉]MgCl〈span〉3〈/span〉·6H〈span〉2〈/span〉O. The mineral is named after Prokopiy Trifonovich Novograblenov, one of the researchers of Kamchatka Peninsula, a teacher, naturalist, geographer and geologist.〈/p〉〈/div〉
    Print ISSN: 0026-461X
    Electronic ISSN: 1471-8022
    Topics: Geosciences
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  • 9
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    CRYSTAL CHEMISTRY OF CANCRINITE-GROUP MINERALS WITH AN AB-TYPE FRAMEWORK: A REVIEW AND NEW DATA. I. CHEMICAL AND STRUCTURAL VARIATIONS (2011)
    Mineralogical Association of Canada
    Details
    Publication Date: 2011-10-01
    Description: Chemical and structural variations of 11 minerals of the cancrinite group having an Al,Si,O framework of the AB type are summarized and discussed. The total number of chemically studied samples is 360 (our data and literature data): cancrinite 192 and 35, vishnevite 21 and 13, cancrisilite 19 and 10, kyanoxalite and oxalate-rich intermediate members of the cancrinite– kyanoxalite series 12 and 0, davyne 10 and 23, depmeierite 2 and 0, balliranoite 1 and 0, hydroxycancrinite 0 and 1, quadridavyne 0 and 10, microsommite 0 and 8, and pitiglianoite 0 and 3. We provide original structural data for nine samples of distinct varieties of cancrinite and one sample of cancrisilite, as well as published structural data on the above-listed minerals. The major topics are the distribution and ratios of extra-framework components, cations (Na+, Ca2+, K+), anions (CO32-, SO42-, Cl-, C2O42-, PO43-) and H2O, with special emphasis on oxalate and phosphate anions. The idealized formula of cancrinite has been refined: Na7Ca[Al6Si6O24](CO3)1.5•2H2O. The solid-solution series with coupled substitutions in the framework and extra-framework portions are discussed, as is the genetic aspect of crystal chemistry of cancrinite-group minerals with a AB-type framework.
    Print ISSN: 0008-4476
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  • 10
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    CRYSTAL CHEMISTRY OF CANCRINITE-GROUP MINERALS WITH AN AB-TYPE FRAMEWORK: A REVIEW AND NEW DATA. II. IR SPECTROSCOPY AND ITS CRYSTAL-CHEMICAL IMPLICATIONS (2011)
    Mineralogical Association of Canada
    Details
    Publication Date: 2011-10-01
    Description: We present a comparative analysis of powder infrared spectra of cancrinite-group minerals with the simplest framework, of AB type, from the viewpoint of crystal-chemical characteristics of extra-framework components. We provide IR spectra for typical samples of cancrinite, cancrisilite, kyanoxalite, hydroxycancrinite, depmeierite, vishnevite, pitiglianoite, balliranoite, davyne and quadridavyne, as well as the most unusual varieties of cancrinite-subgroup minerals (Ca-deficient cancrinite, H2O-free cancrinite, intermediate members of the series cancrinite – hydroxycancrinite, cancrinite–cancrisilite, cancrinite– kyanoxalite, K-rich vishnevite, S2-bearing balliranoite). Samples with solved crystal structures are used as reference patterns. Empirical trends and relationships between some parameters of IR spectra, compositional characteristics and unit-cell dimensions are obtained. The effect of Ca content on stretching vibrations of CO32- is explained in the context of the cluster approach. The existence of a hydrous variety of quadridavyne is demonstrated.
    Print ISSN: 0008-4476
    Topics: Geosciences
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