ISSN:
1572-8854
Source:
Springer Online Journal Archives 1860-2000
Topics:
Geosciences
,
Physics
Notes:
Abstract The structure of the compound obtained by reaction of AlCl3-promotedm-xilene with 2,6-pyridine dicarbonyldichloride in dichloromethane has been investigated by X-ray diffraction methods. The compound is monoclinic, space groupP21/c,a=13.907(2),b=17.247(3),c=12.042(2) Å,β=109.75(4)°. The structure was solved by direct methods and refined by full matrix least-squares to a finalR=6.37 for 3718 independent observed reflections [I〉2σ(I)]. The structure of the compound enables an understanding of the chemical pathway of the synthesis process.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF01160987
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