ISSN:
1573-5001
Keywords:
build-up curves
;
heteronuclear cross-polarization
;
normalization of NOE
;
selective NOE
Source:
Springer Online Journal Archives 1860-2000
Topics:
Biology
,
Chemistry and Pharmacology
Notes:
Abstract A novel one-dimensional NOE experiment is presented where a selected proton is excited by two-way heteronuclear cross- polarization between protons and nitrogen-15 or carbon-13. The utility of the method is demonstrated for a sample of 15N labeled human ubiquitin. Inter- and intra-residue NOEs are clearly observed in a very time-effective manner. The signal intensities can be easily normalized.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1023/A:1008307012647
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