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  • diiodo  (2)
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  • 1
    Electronic Resource
    Electronic Resource
    Crystal structure of [WI2(CO)3{P(OMe)3}2] (1998)
    Springer
    Journal of chemical crystallography 28 (1998), S. 639-643 
    Details
    ISSN: 1572-8854
    Keywords: Tungsten(II) ; diiodo ; carbonyl ; trimethylphosphite ; crystal structure
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract [WI2(CO)3{P(OMe)3}2]crystallizes in the orthorhombic space group Pca21, with a = 26.924(5), b = 10.726(2), c = 14.136(3) Å, and Z = 8. There are two molecules in the asymmetric unit, the metal atoms in each case being seven-coordinate with a capped fac-(CO)3 octahedral geometry. The molecular dimensions in the two molecules are nearly identical. The W–P distance to the capping atom 2.397 Å (average) is significantly shorter than the other W–P distance, 2.525 Å (average).
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1022469211406
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  • 2
    Electronic Resource
    Electronic Resource
    Crystal structure of [WI2(CO)2{P(OiPr)3}(η2-EtC2Et)] (2000)
    Springer
    Journal of chemical crystallography 30 (2000), S. 181-184 
    Details
    ISSN: 1572-8854
    Keywords: tungsten(II) ; diiodo ; dicarbonyl ; triisopropylphosphite ; 3-hexyne ; crystal structure
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract [WI2(CO)2{P(OiPr)3}(η2-EtC2Et)] crystallizes in the monoclinic space group P21/n, with a = 11.101(12), b = 16.272(18), c = 14.892(17) Å, β = 93.27(1), Z = 4. The geometry can be considered to be pseudo-octahedral, with the 3-hexyne ligand occupying one site, with two iodo-groups, and the P(OiPr)3 ligand completing the equational plane of ligands, with two trans-carbonyl groups occupying the axial sites.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1009531014474
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    Paper (German National Licenses)
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