ISSN:
0749-1581
Keywords:
Assignment strategy
;
K3 serotype
;
Polysaccharide
;
Porphyrin
;
NMR
;
Phase cycling
;
Reverse correlation
;
Two-dimensional
;
Heteronuclear multiple quantum
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The practical aspects of proton-detected heteronuclear shift correlation spectroscopy are described in detail, with emphasis on the precautions necessary to obtain efficient suppression of signals from protons that are not coupled to 13C. The experiment has been used to assign the quaternary carbon signals of a porphyrin and to resolve the proton spectrum of the K3 serotype polysaccharide.
Additional Material:
7 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260261011
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