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  • 1
    Electronic Resource
    Electronic Resource
    A Convenient Synthetic Route to Polyether-Tagged Cyclam Ligands andTheir Nickel Derivatives (1999)
    Weinheim : Wiley-Blackwell
    Liebigs Annalen 1999 (1999), S. 3257-3261 
    Details
    ISSN: 1434-193X
    Keywords: Cyclam ; PEO ; Nickel ; Electrochemistry ; Macrocyclic compound ; Chemistry ; General Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A specific strategy is described for the synthesis of stable polyethylene oxide tagged tetraazamacrocycles (PEO-cyclam) in five steps (overall yields for 12 and 13 48% and 22%, respectively). Various attempts via classical pathways demonstrated: (i) the low reactivity of PEO derivatives, and (ii) the necessity of a stabiliser arm between the cyclam and the PEO chain. Nickel complexes have been prepared and characterised by electrochemistry.
    Additional Material: 1 Tab.
    Type of Medium: Electronic Resource
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