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Determination of biogenic quaternary ammonium compounds on fused silica capillary columns with a splitless injector as a chemical reactor/pyrolysis chamber (1984)

Findeis, P. M. ; Farwell, S. O.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 7 (1984), S. 19-24

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ISSN: 0935-6304

Keywords: Gas chromatography ; Capillary, fused silica ; Splitless injection ; Flash derivatization ; Quaternary ammonium compounds ; Acetylcholine ; Biogenic amines ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: A conventional splitless injector is used as a pyrolysis chamber or chemical reactor for the N-demethylation of acetylcholine and other choline esters. The novel uses of 2-aminoethanol as a N-demethylation reagent in splitless injection and bonded-phase fused silica capillary columns in the separation of the tertiary amine derivatives of choline esters are described. A comparison is made between non-polar and moderately polar fused silica capillary columns in the separation of choline esters.

Additional Material: 4 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jhrc.1240070104

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