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61Ni NMR spectroscopy of di- and tricarbonylnickel complexes (1995)

Behringer, Klaus D. ; Blümel, Janet

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 33 (1995), S. 729-733

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ISSN: 0749-1581

Keywords: NMR ; 61Ni NMR ; solenoid probehead ; carbonylnickel phosphine complexes ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Di- and tricarbonylnickel phosphine complexes (22) were prepared and their liquid-state 61Ni NMR spectra were recorded with the use of special solenoid glass sample tubes and a solenoid probehead, which are described. The acquired chemical shifts δ(61Ni), linewidths v1/2(Ni), relaxation times T1 and coupling constants 1J(61Ni,31P) are discussed with reference to the electronegativity of the substituents at the phosphine ligands and the Tolman angle θ of the latter.

Additional Material: 4 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260330907

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