ISSN:
0749-1581
Keywords:
1H NMR
;
13C NMR
;
Bile salts
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
1H and 13C NMR assignments of sodium chenodeoxycholate in aqueous solution were obtained for three different bile salt concentrations. 1H and 13C NMR chemical shifts of sodium chenodeoxycholate and deoxycholate show slight concentration dependence due to micelle formation. Opposite trends in chemical shifts changes for α- and β-protons cause polarization of the steroid nucleus.
Additional Material:
2 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/mrc.1260320206
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