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Characterization of octadecylsilica stationary phases by spectroscopic methods (1993)

Jinno, K. ; Wu, J. ; Ichikawa, M. ; [et al.]

Springer

Chromatographia 37 (1993), S. 627-634

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ISSN: 1612-1112

Keywords: Column liquid chromatography ; ODS phases ; NMR and FTIR characterization ; Stationary phase functionality

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Summary Two spectroscopic methods, solid state NMR and diffuse reflectance FTIR, have been used in conjunction with liquid chromatographicretention data to identify and distinguish the functionality of octadecylsilica (ODS) stationary phases. NMR and FTIR spectra are indicative of various features of the different functionalities of the phases and this information can be used to elucidate the configuration of the organosilyl moiety in the ODS on the silica surface and explain why DSS phases have different molecular shape (mainly planarity) recognition capability.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF02274114

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