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Determination of extracolumn effects in recycle gas chromatography with capillary columns (1988)

Roberts, D. ; Bertsch, W.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 11 (1988), S. 783-787

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ISSN: 0935-6304

Keywords: Gas chromatography, GC ; Recycle GC ; Peak distortion ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Extracolumn band broadening in multidimensional systems utilizing flow switching is clearly undesirable. In certain cases, i.e. capillary recycle gas chromatography, the success of an experiment is contingent on the minimization of pre- and post-column dispersion of the peaks. Knowledge of these sources of peak distortion is necessary to optimize the experimental design. A system that extracts statistical parameters from real chromatographic peaks is discussed and used to evaluate band broadening in a capillary recycle experiment.

Additional Material: 6 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jhrc.1240111107

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