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  • Capillary gas chromatography  (3)
  • Engineering  (3)
  • Numerical Methods and Modeling  (3)
  • Wiley-Blackwell  (6)
  • American Society of Hematology
  • 1
    Electronic Resource
    Electronic Resource
    Effect of viscosity on stationary phase stability in capillary column gas chromatography (1982)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 5 (1982), S. 413-416 
    Details
    ISSN: 0935-6304
    Keywords: Capillary gas chromatography ; Stationary phase stability ; Stationary phase viscosity ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: With recent advances in column technology it is now possible to prepare highly efficient, very inert, and thermally stable capillary columns coated with nonpolar polysiloxane stationary phases. Unfortunately, the same degree of success has not been achieved for some of the more polar polysiloxane phases. A parameter that has been studied little in the past in relation to stationary phase film stability is the viscosity of the stationary phase. In this paper the efficiency and stability of coated columns are correlated to the viscosity of the phase. Due to their structure, the viscosity of the phenyl-containing polysiloxanes change rapidly with temperature and hence, thin-film coatings are not stable at elevated temperatures. By using high viscosity phenyl-containing methylphenylpolysiloxanes which were recently synthesized, efficient and stable columns have been prepared.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240050804
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  • 2
    Electronic Resource
    Electronic Resource
    Multi-element selective radio frequency plasma detector for capillary gas chromatography (1988)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 11 (1988), S. 75-81 
    Details
    ISSN: 0935-6304
    Keywords: Capillary gas chromatography ; Element selective detection ; Radio frequency plasma ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A radio frequency plasma detector for element specific detection in gas chromatography is described. The detector is comprised of a radio frequency (300 kHz) discharge between electrodes in helium, and utilizes a low-resolution emission spectrometer to monitor selected spectral emission lines produced when the helium discharge decomposes and excites the atomic constituents in the chromatographic column effluent. The spectrometer is tuned to an atomic emission line in the near-infrared portion of the spectrum, and the emission intensity from the discharge region of a selected line is used to monitor the concentration of the element producing that line. Acceptable detector sensitivity was achieved by the use of a high-throughput optical system. Selectivity was achieved by a combination of correct line selection, plasma and carrier gas purification, and plasma gas doping.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240110120
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  • 3
    Electronic Resource
    Electronic Resource
    Azo compounds for free radical crosslinking of polysiloxane stationary phases (1983)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 6 (1983), S. 371-374 
    Details
    ISSN: 0935-6304
    Keywords: Free radical crosslinking ; Capillary gas chromatography ; Azo compounds ; Nonextractable Polysiloxane stationary phases ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: There has been much effort spent in recent years developing the technology for free radical crosslinking of polysiloxane polymers to prepare capillary columns coated with thermally stable and nonextractable stationary phases. Organic peroxides have been used extensively as the free radical initiators for the in situ polymerization of the stationary phases. However, these peroxides adversely affect the phase polarity and column activity. Seven azo compounds were studied for crosslinking efficiency. Azo compounds can be used as free radical initiators to prepare nonextractable stationary phases without the adverse effects caused by peroxides.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240060705
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  • 4
    Electronic Resource
    Electronic Resource
    General approach to automatic generation of quadrilaterals on three-dimensional surfaces (1998)
    Chichester : Wiley-Blackwell
    Communications in Numerical Methods in Engineering 14 (1998), S. 609-620 
    Details
    ISSN: 1069-8299
    Keywords: quadrilateral finite-element generation ; three-dimensional surfaces ; CAD/CAM interface ; topological information generation ; node sampling on edges ; Engineering ; Numerical Methods and Modeling
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: In this paper, a general approach to automatic generation of quadrilaterals on three-dimensional surfaces is presented. The approach is based on the mapping method for surface meshing and the looping method for generation of quadrilaterals on the mapped plane. Several schemes including a coedge treatment scheme, an allowable tolerance and distance scheme, a multipatch treatment scheme with new mapping functions and a remapping scheme are proposed. Several realistic application examples are given, which show the generality of the presented approach. © 1998 John Wiley & Sons, Ltd.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    An efficient method of solving the Navier-Stokes equations for flow control (1998)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 41 (1998), S. 1133-1151 
    Details
    ISSN: 0029-5981
    Keywords: flow control ; numerical solution of Navier-Stokes equation ; Karhunen-Loève Galerkin procedure ; Engineering ; Numerical Methods and Modeling
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: A new method of solving the Navier-Stokes equations efficiently by reducing their number of modes is proposed in the present paper. It is based on the Karhunen-Loève decomposition which is a technique of obtaining empirical eigenfunctions from the experimental or numerical data of a system. Employing these empirical eigenfunctions as basis functions of a Galerkin procedure, one can a priori limit the function space considered to the smallest linear subspace that is sufficient to describe the observed phenomena, and consequently reduce the Navier-Stokes equation defined on a complicated geometry to a set of ordinary differential equations with a minimum degree of freedom. The present algorithm is well suited for the problems of flow control or optimization, where one has to compute the flow field repeatedly using the Navier-Stokes equation but one can also estimate the approximate solution space of the flow field based on the range of control variables. The low-dimensional dynamic model of viscous fluid flow derived by the present method is shown to produce accurate flow fields at a drastically reduced computational cost when compared with the finite difference solution of the Navier-Stokes equation. © 1998 John Wiley & Sons, Ltd.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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  • 6
    Electronic Resource
    Electronic Resource
    Quadrilateral finite-element generation and mesh quality control for metal forming simulation (1997)
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 40 (1997), S. 4059-4075 
    Details
    ISSN: 0029-5981
    Keywords: optimal quadrilateral finite-element generation ; improved looping method ; optimal nodal placement ; geometrical quality index function ; automatic forging simulation ; metal forming ; Engineering ; Numerical Methods and Modeling
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mathematics , Technology
    Notes: An improved looping method for quadrilateral finite element generation, effective especially for automatic metal forming simulation, was presented in this paper. A new splitting criterion to improve the conventional looping method, an artificial boundary scheme to reduce mesh transition regions and an optimal nodal placement scheme to enhance local and global mesh quality were introduced in the standpoint of metal forming engineering. Various application examples were given, which show versatility and applicability of the presented approaches and the developed mesh generator. Application examples including automatic computer simulation of a forging process showed that the presented approaches are powerful for metal forming simulation. © 1997 John Wiley & Sons, Ltd.
    Additional Material: 15 Ill.
    Type of Medium: Electronic Resource
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