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  • Articles  (6)
  • International Union of Crystallography (IUCr)  (3)
  • American Chemical Society (ACS)  (1)
  • Geological Society of America (GSA)
  • Mineralogical Society of Great Britain and Ireland
  • 1
    Electronic Resource
    Electronic Resource
    Structure Refinement of Y2Ru2O7 by Neutron Powder Diffraction (1995)
    Oxford [u.a.] : International Union of Crystallography (IUCr)
    Acta crystallographica 51 (1995), S. 790-792 
    Details
    ISSN: 1600-5759
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1107/S0108270194013168
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    The Performance of the Australian Powder Diffractometer at the Photon Factory, Japan (1995)
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 28 (1995), S. 513-517 
    Details
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Australian scientists have built and installed an X-ray powder diffractometer of an unusual design on the Australian beamline at the Photon Factory synchrotron-radiation facility within the National Laboratory for High Energy Physics (KEK), Tsukuba, Japan. The diffractometer is a Debye–Scherrer camera of 0.573 m radius. The place of the cylindrical film in a conventional camera of this type is taken by image plates. To minimize scattering and absorption by air, the instrument can be evacuated. The instrument is now in operation and has been tested with a specimen of the rutile phase of TiO2. This material has been thoroughly studied previously and it has been demonstrated that time-of-flight neutron powder diffraction, conventional neutron powder diffraction, single-crystal neutron diffraction and single-crystal X-ray diffraction lead to a consistent set of values for the anisotropic thermal parameters and the one positional parameter. The powder specimen of rutile for use at KEK was diluted with gum tragacanth and inserted into a glass capillary of 0.5 mm diameter. The beam from the synchrotron is incident on a silicon (111) channel-cut monochromator. Data were collected to ±165°2θ at wavelengths of 0.62, 1.10, 1.54 and 1.90 Å. The exposure time for each data set was 10 min. The resolution of the instrument agrees with theoretical prediction and is such that the full width at half-maximum of a reflection varies from 0.04° at 20°2θ to 0.2° at 160°2θ for a wavelength of 1.54 Å. The intensity from a 10 min exposure is more than sufficient for Rietveld refinement (Rexp 〈 1%).
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1107/S0021889894014627
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  • 3
    Electronic Resource
    Electronic Resource
    Structural Studies of Rutile-Type Metal Dioxides (1997)
    Copenhagen : International Union of Crystallography (IUCr)
    Acta crystallographica 53 (1997), S. 373-380 
    Details
    ISSN: 1600-5740
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Chemistry and Pharmacology , Geosciences , Physics
    Notes: The structures of the four metal dioxides GeO2, SnO2, RuO2 and IrO2 (germanium, tin, ruthenium and iridium dioxides, respectively) have been redetermined by Rietveld refinement from neutron diffraction powder data. The four dioxides all adopt the rutile-type structure, space group P42/mnm (no. 136), with a = 4.4066 (1), 4.7374 (1), 4.4968 (2) and 4.5051 (3), c = 2.8619 (1), 3.1864 (1), 3.1049 (1) and 3.1586 (2) Å, and x = 0.3060 (1), 0.3056 (1), 0.3053 (1) and 0.3077 (3), respectively. These results are compared with those for other metal dioxides that adopt the rutile structure and trends in structural and thermal vibrations for a series of 11 metal dioxides which adopt the rutile-type structure are described.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1107/S0108768197001468
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  • 4
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    Differential Effects and Potential Adverse Outcomes of Ionic Silver and Silver Nanoparticles in Vivo and in Vitro (2014)
    American Chemical Society (ACS)
    Details
    Publication Date: 2014-04-02
    Description: Environmental Science & Technology DOI: 10.1021/es4042258
    Print ISSN: 0013-936X
    Electronic ISSN: 1520-5851
    Topics: Chemistry and Pharmacology , Energy, Environment Protection, Nuclear Power Engineering
    Published by American Chemical Society (ACS)
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  • 5
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    Magma storage, differentiation, and interaction at Lake City caldera, Colorado, USA (2016)
    Geological Society of America (GSA)
    Details
    Publication Date: 2016-04-29
    Description: Rocks from the 23 Ma Lake City caldera show diverse chemical affinities attesting to a complex magmatic system beneath the caldera. Field and geochemical data from ignimbrites and intrusions constrain magma storage and magma interactions during the formation of the caldera. Two geochemically distinct magma batches erupted during caldera formation: batch A, consisting of rhyolites and trachytes, and batch B, consisting of dacites and trachyandesites. The ignimbrites of the Lower, Middle, and Upper Sunshine Peak Tuff represent the bulk of erupted batch A magma, with an increasing proportion of trachyte to rhyolite as the eruption progressed. Overall, the observed trends of major and trace elements are consistent with the sequential eruption of a magmatic system with a rhyolitic upper portion and trachytic lower portion. The Middle Sunshine Peak Tuff contains two distinct types of pumice clast, while the Upper Sunshine Peak Tuff contains four distinct pumice clast types, with one type chemically related to batch B magma. The link between the rhyolite and trachyte of batch A is supported by major- and trace-element geochemical modeling of an initially trachytic magma that fractionated and was subjected to crystal/melt segregation following 50%–60% crystallization. Compositional gaps and chemical heterogeneity in the bulk ignimbrite composition show that the proportions of these different magma types varied significantly during eruption. We propose that the fractionating batch A and B magmas formed distinct magma pods, some containing residual magma mush, that were tapped during different phases of caldera formation. After collapse, dacite lavas of batch B were erupted concurrent with resurgent uplift from shallow intrusion of both residual mingled batch A and batch B magma. In summary, our observations suggest (1) a complex magma chamber geometry from two fractionating magma batches, and (2) magma replenishment and accelerated periods of magma reorganization in the shallow magma plumbing system during a single caldera cycle at Lake City.
    Print ISSN: 0016-7606
    Electronic ISSN: 1943-2674
    Topics: Geosciences
    Published by Geological Society of America (GSA)
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  • 6
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    Copper substitution alone and in the presence of chromium, zinc, cadmium and lead in goethite (α-FeOOH) (2009)
    Mineralogical Society of Great Britain and Ireland
    Details
    Publication Date: 2009-09-01
    Description: A series of Cu-substituted goethites, single and co-substituted with Cr, Zn, Cd and/or Pb was prepared, having molar ratios equal to 2.00, 3.33 and 5.00 mol%. All the samples contained only goethite, except Cu-, (Cu,Zn)- and (Cu,Pb)-samples synthesized at 5.00 mol% where hematite was also formed. The presence of Cr/Cd suppressed the hematite-forming effects of Cu. The general sequence of metal entry into the single-metal-substituted goethites was Zn = Cr 〉 Cd 〉 Cu 〉 Pb and in di- (5.00 mol%) and tri- (3.33 mol%) metal-substituted goethites was Cu 〉 Zn 〉 Cd 〉 Cr 〉〉 Pb. Cu incorporation increased all the unit-cell parameters in single-metal-substituted goethite, and these parameters increased in combination with other metals as follows: Cd 〉 Zn 〉 Cr 〉 Pb in the multimetal-substituted goethites. The Cu-substituted goethite dissolved faster than pure goethite. Co substitutions of Cr/Pb reduced the dissolution rate (kFe), while substitutions of Cd/Zn increased kFe.
    Print ISSN: 0009-8558
    Electronic ISSN: 1471-8030
    Topics: Geosciences
    Published by Mineralogical Society of Great Britain and Ireland
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