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Reduction-Nitridation Synthesis of Titanium Nitride Nanocrystals (2003)

Yang, Xiaogang ; Li, Cun ; Yang, Lihua ; [et al.]

Westerville, Ohio : American Ceramics Society

Journal of the American Ceramic Society 86 (2003), S. 0

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ISSN: 1551-2916

Source: Blackwell Publishing Journal Backfiles 1879-2005

Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics

Notes: Titanium nitride (TiN) particles (8 nm) were prepared via a reduction-nitridation route in an autoclave at 500°C, using TiCl4, NH4Cl, and metal Na as reactants. X-ray powder diffraction indicated that the product was a NaCl-type of TiN with a cell constant a= 4.242 Å. Transmission electron microscopy images showed that the TiN particles were 5–10 nm. Raman spectra showed the defect-induced first-order shifts in the TiN nanocrystals.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1111/j.1151-2916.2003.tb03308.x

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