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  • 1
    Electronic Resource
    Electronic Resource
    Carriers for drugs and enzymes based on copolymers of allyl glycidyl ether with acrylamide (1982)
    New York : Wiley-Blackwell
    Die Makromolekulare Chemie 183 (1982), S. 781-788 
    Details
    ISSN: 0025-116X
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Copolymerization of acrylamide with allyl glycidyl ether yielded water soluble polymers containing an epoxy group; addition of a crosslinking agent, N,N′-methylenebis(acrylamide), to the copolymerization mixtures resulted in the formation of similar though water insoluble polymers. Condensation of a potent beta-adrenergic antagonist Alm—H, which contains a reactive amino group, with a polymer containing an epoxy group yeilded a pharmacologically active polymer. The polymer containing the epoxy group was also converted, by reaction with sodium thiosulfate and subsequent reduction, into a mecapto groups containing polymer which was also water soluble. The latter polymer was converted by condensation with a beta-adrenergic antagonist Alm—COCH2Br, which contains a reactive bromoacetamido group, into a pharmacologically active polymer.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/macp.1982.021830403
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  • 2
    Electronic Resource
    Electronic Resource
    The determination of the isotacticity of polypropylene in the 90-100% range by infrared spectroscopyPresented as a paper before the Meeting of the American Chemical Society Division of Polymer Chemistry, September 1963, in New York City. At that time this laboratory was the Research Center of the Spencer Chemical Company. (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 417-425 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: An infrared method has been developed for the determination of the isotacticity of polypropylene in the 90-100% range. The method requires the annealing of thin films at 165-167°C. for 3 hr. in an inert atmosphere, followed by slow cooling to room temperature. For approximate answers the ratio of the intensity of the 10.00 μ band to that of the 10.27 μ band can be reported as the fraction of isotactic material. Better results are obtained, however, by using Figure 2 as a calibration curve and reading the values from it.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070130302
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  • 3
    Electronic Resource
    Electronic Resource
    Effect of type and amount of comonomer on the properties of four copolymers of ethylene (1966)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 6 (1966), S. 5-14 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The plastics industry is now coming to realize that copolymers are unique thermoplastics which have broad areas of application. It is believed that ethylene-methyl acrylate copolymers of 2 melt index may be extrusion coated to paper by a cap-coat process or by use of a chill roll with an adhesive coating. Copolymers of ethylene and vinyl monomers can be made into film by the same methods used for polyethylene. Methyl acrylate and methyl methacrylate copolymers may be processed on a wide range of molding equipment. Table VII in the article gives a list of applications for each polymer, along with expected physical properties.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760060103
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  • 4
    Electronic Resource
    Electronic Resource
    Photoresist development by plasma (1980)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 20 (1980), S. 1093-1096 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Over the past several years the semiconductor industry has placed major efforts into replacing wet processes with dry processes in fabricating electronic devices. Plasma photoresist stripping, plasma cleaning, and other dry etching techniques have replaced wet methods in many product lines. One area that has received little mention but which is vital toward achieving a totally dry manufacturing process is the dry development of photoresist. One production applicable plasma developable photoresist (PDF) process, using a proprietary resist formulation, is reported. Plasma process characterization, such as end point detection, development latitude, and mechanism are discussed. Included also are development temperature, batch film uniformity, and resolution currently obtainable with the PDF process.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760201611
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  • 5
    Electronic Resource
    Electronic Resource
    Transparent barrier resins with high nitrile content (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 2567-2577 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The effect of 30-49 wt-% nitrile group content on the properties of copolymers is demonstrated. The nitrile is furnished by either acrylonitrile or methacrylonitrile. The exceptional resistance of such high nitrile content resins to the passage of gases and of solvents is shown and variations therein demonstrated for different comonomers. Transparent, tough, grafted polymers of good color are described which retain these properties. These qualities, combined with low second-order transition temperatures and adequate heat deflection temperatures, provide polymers of interest wherever containment and barrier are desired. Bottles, thermoformed containers, etc., could benefit from the use of some of the polymers described.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070131205
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  • 6
    Electronic Resource
    Electronic Resource
    Binary and ternary blends of poly(vinyl chloride), hytrel, and a polyurethane (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 3467-3473 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Binary blends of poly(vinyl chloride) and a poly(ether urethane) containing 20 and 40 weight percent, respectively, of poly(vinyl chloride) have been prepared by solution blending from tetrahydrofuran and their degree of mixing investigated using dynamic mechanical analysis. In the polyurethane, transitions were found at -19°C and -119°C. The former was attributed to the glass transition and the latter to a Schatzki type of motion of the polyether sequences. This latter transition occurred at a temperature which is higher than the literature value for the low temperature transition in poly(tetrahydrofuran), which is equivalent to the polyether sequence in the polyurethane. This discrepancy is attributed to the influence of neighboring hard segments present because of incomplete segmental phase separation of the polyurethane. For the blends only one very broad transition was observed, indicating that there was substantial mixing of these two polymers. Three ternary blends were prepared, also by solution blending, containing poly(vinyl chloride), Hytrel, and the polyurethane in the ratios 1:1:1, 1:2:1, and 2:1:1, respectively. In the first two blends there was clear evidence of phase separation. It was only in the 2:1:1 blend that an apparently significantly compatible material resulted.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070261025
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  • 7
    Electronic Resource
    Electronic Resource
    Use of gas-liquid chromatography in the analysis of rigid polyurethane foam polyols (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 1297-1307 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Detailed characterization of the low molecular weight polyols used as intermediates in rigid polyurethane foam production has not been feasible to date. Gas-liquid chromatography of the trimethylsilyl ether derivatives of the polyols now offers a more complete picture of polyol composition, particularly with regard to the molecular weight distribution. The data may be interpreted on a semiquantitative basis. The study of processing variables in polyol manufacture, detection of impurities and analysis of unknown polyols or those based on mixed initiators may all be facilitated by use of this GLC technique.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070130617
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  • 8
    Electronic Resource
    Electronic Resource
    Polymeric systems for acoustic damping. III. Blends of poly(vinyl chloride), segmented poly(ether ester), and poly(methyl acrylate) (1981)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 26 (1981), S. 3487-3491 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A solution blend of poly(vinyl chloride) and a segmented poly(ether ester) and blends containing these two polymers plus poly(methyl acrylate) were investigated by dynamic mechanical analysis and electron microscopy. The binary blend, which contained 75% by weight of the poly(ether ester), showed only one loss peak, but also evidence of some phase separation. It is believed that the polyether sequences of the poly(ether ester) are extensively mixed with poly(vinyl chloride). Poly(methyl acrylate) was added to spread the damping range and produce a material of potential use as an acoustic damper. It is evident from both electron microscopy and dynamic mechanical analysis that poly(methyl acrylate) is substantially incompatible in the other polymers.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1981.070261027
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  • 9
    Electronic Resource
    Electronic Resource
    An experimental and theoretical study of the transmission function of a commercial hemispherical electron energy analyserPaper presented at the International Conference on Quantitative Surface Analysis held at the National Physical Laboratory, Teddington, UK, 24-25 November 1981. (1982)
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 4 (1982), S. 220-226 
    Details
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The electron energy analyser transmission (peak area/incident current) of a VG Scientific ESCALAB has been measured as a function of kinetic energy, analyser energy and source position for a point source of electrons in the sample plane (produced using a specially designed mini electron gun). Results have been obtained in both CAE (constant analyser energy) and CRR (constant retard ratio) modes. The results are extrapolated to give the energy dependence of the analyser transmission for an extended current source, such as encountered in routine XPS analysis applications. A detailed theoretical study explains the rationale behind this data extrapolation and predicts an analyser transmission in fair agreement with experimental results, possible causes for the discrepancies between theory and experiment are discussed.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/sia.740040509
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  • 10
    Electronic Resource
    Electronic Resource
    Poly-α-cyanostyrene (1965)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A: General Papers 3 (1965), S. 1527-1533 
    Details
    ISSN: 0449-2951
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The monomer α-cyanostyrene polymerized at a very slow rate under the influence of free-radical initiators. Rapid polymerization to high molecular weight material was achieved by using anionic initiators (tri-n-butylphosphine and tetrakisdimethylaminotitanium). The polymer made at -78°C. was colorless, fusible, soluble, and had a number-average molecular weight of over 5,000. The polymer prepared at 0°C. was brown, insoluble, and infusible. None of the polymer showed order in the x-ray diagram. The rate of dimerization of α-cyanostyrene under a wide variety of conditions was measured. Two new derivatives of the intermediate, 3-(N,N-dimethylamino)-2-phenylpropionitrile were prepared: the methiodide, m.p. 242-245°C. (decomp.), and the picrate, m.p. 116.5-117.5°C.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1965.100030420
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