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  • ASTRONOMY  (2)
  • Small molecular weight amines and diamines  (1)
  • Chaperone
  • Condensed Matter: Electronic Properties, etc.
  • 1985-1989  (3)
  • 1
    Electronic Resource
    Electronic Resource
    Quantitative analysis of ethylenediamine in plasma by capillary column gas chromatography (1986)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 9 (1986), S. 548-554 
    Details
    ISSN: 0935-6304
    Keywords: Gas liquid chromatography (GLC) ; Fused silica capillary columns ; Alkali flame ionization detection (AFID) ; Mass spectrometry (MS) ; Quantitation in human serum ; Ethylenediamine ; Aminophylline ; Small molecular weight amines and diamines ; m-Toluoyl derivatives ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: A specific and sensitive method for the determination of ethylenediamine in human plasma is described. The aqueous sample is treated with m-toluoyl chloride, yielding the N,N′-bis(m-toluoyl) derivative of the diamine, which is extracted into dichloromethane and quantitated after “on column” methylation by capillary gas liquid chromatography with alkali flame ionization detection. The corresponding derivative of putrescine serves as internal standard. The assay is reproducible and calibration curves are linear over the concentration range 0.05 to 10 μg · ml-1. The lower detection limit is about 10 ng · ml-1. The structures of the compounds of interest eluting from the capillary column are examined by gas liquid chromatography/mass spectrometry. The assay has been applied to the analysis of ethylenediamine in plasma following the administration of aminophylline and ethylenediamine in a cross-over study to patients with bronchopulmonary diseases. The method also proves suitable for measuring other primary and secondary amines and diamines in aqueous solutions by gas liquid chromatography.
    Additional Material: 7 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/jhrc.1240091002
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    Paper (German National Licenses)
    Fulltext
  • 2
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    Optical observations of SN 1987D in UGC 7370 (1987)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: This paper presents optical photometry and spectroscopy of SN 1987D, a Type Ia supernova in the nearby galaxy UGC 7370, during the period immediately subsequent to its discovery. The distance modulus of the galaxy, independently determined by the redshift and the Tully-Fisher (1977) relation, is 32.3 + or - 1.0. The maximum brightness of SN 1987D was V about 13.2 and occurred on April 18, 1987, + or - 4 days; the absolute luminosity is about 0.6 mag brighter than the average for SNe Ia. The spectrum of SN 1987D is typical of SNe Ia, but the expansion velocity (9600 km/s) is considerably lower than average.
    Keywords: ASTRONOMY
    Type: Astronomical Society of the Pacific, Publications (ISSN 0004-6280); 99; 1167-117
    Format: text
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    NASA TECHNICAL REPORTS
  • 3
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    X-ray observations of the bright quasar survey (1986)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: Using the Einstein Observatory, X-ray observations of about 80 percent of the quasars in the Bright Quasar Survey located outside the declination range defined by 30 and 60 deg. X-ray emission has been detected above the 3-sigma level for 57 out of 66 quasars observed. This paper describes observations and data reduction and provides a summary of the more detailed analyses and discussion contained in the two accompanying papers (Schmidt and Green 1986, Avni and Tananbaum 1986).
    Keywords: ASTRONOMY
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 305; 57-67
    Format: text
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    NASA TECHNICAL REPORTS
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