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  • 1
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    Voltammetric studies of porous molybdenum electrodes for the alkali metal thermoelectric converter (1986)
    In:  Other Sources
    Details
    Publication Date: 2011-08-19
    Description: Voltammetry of partially oxidized porous molybdenum alkali metal thermoelectric converter (AMTEC) electrodes from about 600 to 1000 K revealed a series of redox processes within the AMTEC operational voltage range which can be used to establish the electronic and ionic conductivities of these electrodes. Improved estimates of the free energies of formation of Na2Mo3O6, NaMoO2, and Na3MoO4 are obtained. Evidence is provided for the slow corrosive attack by Na2MoO4 on molybdenum. The ionic conductivity of Na2MoO4 is found to be sufficiently large at temperatures of greater than 700 K to explain the observed electrochemical phenomena in addition to the enhanced sodium transport in AMTEC electrodes below the freezing point of Na2MoO4.
    Keywords: ELECTRONICS AND ELECTRICAL ENGINEERING
    Type: Electrochemical Society, Journal (ISSN 0013-4651); 133; 2253-225
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  • 2
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    CNO abundances in novae ejecta (1985)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: Isotope production, particularly CNO, which are enhanced in novae events and the interstellar medium (ISM) by novae are discussed in terms of emission-line data taken a few weeks after novae events. The emission-line abundances emerge only after the fading of absorption spectrum, and are also detectable in thin shells which sometimes, though rarely, form after novae. CNO abundances in these shells are equivalent to those observed in fading novae, with CNO/H ratios being 100 times solar values. Possible heavy element production pathways in the events and their shrinking are discussed, along with observation techniques for detecting CNO isotopes through absorption data on atomic transitions in novae ejecta and the ISM.
    Keywords: ASTROPHYSICS
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  • 3
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    The role of oxygen in porous molybdenum electrodes for the alkali metal thermoelectric converter (1986)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: A model for chemical reactions in porous molybdenum electrodes is presented which is based on thermochemical and kinetic data, known sodium-molybdenum-oxygen chemistry, X-ray diffraction analysis of molybdenum and molybdenum oxide electrodes, and the electrochemical behavior of the cell. Enhanced sodium transport through the electrode in its optimum performance state is found to be due to the high sodium ion conductivity of molten Na2MoO4 in the pores, and the electrical conduction to the molybdenum matrix by Na2Mo3O6. The decline of electrode performance is shown to be due to a combination of loss mechanisms for the Na-Mo-O compounds including reduction at short circuit, disproportionation of Na2Mo3O6 at open circuit, and the evaporation of Na2MoO4 at elevated temperature. It is suggested that operation of the cell at moderate voltage of about 0.5 V corresponding to maximum power may be a more stable condition for the porous electrode than open-circuit stand or short-circuit, where degradation reactions are heightened.
    Keywords: ENERGY PRODUCTION AND CONVERSION
    Type: Electrochemical Society, Journal (ISSN 0013-4651); 133; 1587-159
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  • 4
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    Ignition of metals and alloys by high-velocity particles (1986)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: The ignition of metals and alloys by impacting high-velocity particles in gaseous oxygen was investigated. A convergent/divergent nozzle was used to accelerate the flowing oxygen, which in turn accelerated the particles to velocities greater than 305 m/s (1000 ft/s). The test sample (target) was placed at the end of the chamber in the flow path. Aluminum 6061, type 316 stainless steel, type 304 stainless steel, and Inconel 718 were ignited with 1600-micron aluminum 2017 particles at elevated temperatures and pressures whereas Monel 400 could not be ignited. The ignition susceptibility of metals and alloys appeared to increase as the inlet pressure, sample temperature, and particle size were increased. Type 304 stainless steel particles required more extreme conditions for ignition of materials than similar sized aluminum particles. The results indicated that ignition and subsequent burning of the particles were required for ignition of the target materials with the possible exception of aluminum 6061.
    Keywords: METALLIC MATERIALS
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  • 5
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    Performance and impedance studies of thin, porous molybdenum and tungsten electrodes for the alkali metal thermoelectric converter (1988)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: Columnar, porous, magnetron-sputtered molybdenum and tungsten films show optimum performance as alkali metal thermoelectric converter electrodes at thicknesses less than 1.0 micron when used with molybdenum or nickel current collector grids. Power densities of 0.40 W/sq cm for 0.5-micron molybdenum films at 1200 K and 0.35 W/sq cm for 0.5-micron tungsten films at 1180 K were obtained at electrode maturity after 40-90 h. Sheet resistances of magnetron sputter deposited films on sodium beta-double-prime-alumina solid electrolyte (BASE) substrates were found to increase very steeply as thickness is decreased below about 0.3-double-prime 0.4-micron. The ac impedance data for these electrodes have been interpreted in terms of contributions from the bulk BASE and the porous electrode/BASE interface. Voltage profiles of operating electrodes show that the total electrode area, of electrodes with thickness less than 2.0 microns, is not utilized efficiently unless a fairly fine (about 1 x 1 mm) current collector grid is employed.
    Keywords: ELECTRONICS AND ELECTRICAL ENGINEERING
    Type: Journal of Applied Electrochemistry (ISSN 0021-891X); 18; 410-416
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  • 6
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    Mechanistic studies related to the safety of Li/SOCl2 cells (1985)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: Mechanistic studies of the reactions in Li-SOCl2 cells have been undertaken to improve understanding of the safety problems of these cells. The electrochemical reduction of 1.5M LiAlCl4/SOCl2 has been investigated using gas chromatography, electron spin resonance spectroscopy, and infrared spectroscopy. Cl2 and S2Cl2 have been identified as intermediates in the reduction of SOCl2, along with a radical species (g/xx/ = 2.004, g/yy/ = 2.016, g/zz/ = 2.008) and the proposed triplet ground-state dimer of this radical. SO2 and sulfur have been identified as products. Based upon these findings, a mechanism for the electrochemical reduction of 1.5M LiAlCl4/SOCl2 has been proposed, and its implications for safety of Li-SOCl2 cells during discharge to +0.5V at 25-30 C are discussed.
    Keywords: ENERGY PRODUCTION AND CONVERSION
    Type: Electrochemical Society, Journal (ISSN 0013-4651); 132; 525-528
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  • 7
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    Oxygen extraction from lunar materials - An experimental test of an ilmenite reduction process (1985)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: The reaction of ilmenite with hydrogen to produce water has been studied experimentally in order to evaluate the effectiveness of using a cold trap to improve yields in a continuous flow process. Yields were enhanced, but not to the degree observed in batch processing systems. The terrestrial simulant used in these studies contained traces of iron sulfide, which released H2S during processing with a deleterious effect on several components of the test system. More sophisticated testing should be undertaken to obtain kinetic data and attention given to the removal of sulfides in the pre-process beneficiation.
    Keywords: INORGANIC AND PHYSICAL CHEMISTRY
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  • 8
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    Blast wave formation of the extended stellar shells surrounding elliptical galaxies (1985)
    In:  Other Sources
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    Publication Date: 2011-08-19
    Description: The existence of stellar shells at large distances from isolated elliptical galaxies is explained in terms of a blast wave associated with an active nucleus phase early in the history of the galaxy. The blast wave sweeps the initial interstellar medium out of the galaxy into an expanding shell which radiatively cools behind its leading shock front. Cooling of the shell following turnoff of the nucleus activity, which keeps the shell photoionized, leads to a brief epoch of star formation which is terminated by heating of the shell from supernovae and UV radiation from massive stars. The stars so formed follow similar, highly radial, bound orbits, moving in phase with each other and spending much of their time near apogalacteum, thus taking on the appearance of a shell. Multiple shells may be produced when conditions allow repeated episodes of shell cooling and supernovae heating to occur in the blast wave.
    Keywords: ASTROPHYSICS
    Type: Astrophysical Journal, Part 1 (ISSN 0004-637X); 291; 80-87
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  • 9
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    IUE observations of the 1981 outburst of nova Cr A (1982)
    In:  Other Sources
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    Publication Date: 2011-08-18
    Description: Low dispersion spectrum observations are analyzed. The light curve of nova Cr A, indicating a moderately fast nova, is presented. Flux calibrated, merged spectrum graphs of April 21, 1981 and September 13, 1981 are presented, demonstrating very strong lines of Al and Si. Additional strong C, Ni, O, and Ne emission lines were identified. Emission lines due to highly ionized species such as Mg VII and Al Vl were observed for short times in May and June 1981. Preliminary analysis of spectra obtained 200 days after maximum indicate that the nebula is still in transition and has not yet reached the nebula state. An over abundance of N and Ne are suggested.
    Keywords: ASTRONOMY
    Type: Advan. in Ultraviolet Astron.; p 478-481
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  • 10
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    Dynamic crystallization experiments on chondrule melts in reduced gravity (1987)
    In:  CASI
    Details
    Publication Date: 2013-08-31
    Description: Chondrules crystallized during the earliest formational history of the solar system; and, if crystal settling and flotation are indicators of crystallization in the presence of gravity, they formed without the influence of gravity. In fact, attempts to duplicate the crystallization history of chondrules in the laboratory have met with limited success, because of the difficulty of comparing objects formed under the influence of gravity with objects that did not. These comparisons are difficult because there are several recognized features introduced by the presence of gravity and no doubt some which are not yet recognized. As a result there are several microscale and macroscale aspects of chondrule petrology which are difficult to understand quantitatively. Most of the features relate to the settling or flotation of early formed crystals. The proposed experiments are briefly described.
    Keywords: MATERIALS PROCESSING
    Type: Experiments in Planetary and Related Sciences and the Space Station; 2 p
    Format: application/pdf
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