ISSN:
1612-1112
Keywords:
Aniline
;
Dimethylthiophosphinyl derivatives
;
Mass fragmentography
;
Environmental analysis
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Summary A method for trace analysis of aniline in water, urine and serum samples is presented. Internal standardisation with d5-aniline, extraction, derivatisation with dimethylthiophosphinic chloride, gas chromatographic separation on a glass capillary column and mass fragmentographic quantitation are essential steps of the analytical procedure. A detection limit of 20 pg/ml in water and 500 pg/ml in urine or serum is achieved.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF02258896
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