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  • 1990-1994  (2)
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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Particle and Particle Systems Characterization 11 (1994), S. 55-62 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Using a computer model based on Lorenz-Mie and generalized Lorenz-Mie theory, various optical confiugurations of a phase-Doppler system were analysed with regard to their suitability for diameter measurements in the sub-micron range. The major concern in this size range is multi-valuedness of the phase-diameter characteristic, the relatively small signal-to-noise ratio obtained with the very low scattered intensity and the small value of the phase difference to be measured. It is shown numerically and by experiment that for particles in a free stream the multi-valuedness and the shot noise need not prohibit measurements in the sub-micron size range. The major source of phase error results from light scattered form objects or material other than the particle inside the measuring volume. Using an optical set-up with nearly counter-propagating incident beams and a large angle between the detectors, measurements were obtained for particle diameters down to 200 nm, and it is estimated that with some improvements in receiver optics measurement down to 100 nm will be possible.
    Additional Material: 20 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Particle and Particle Systems Characterization 11 (1994), S. 63-72 
    ISSN: 0934-0866
    Keywords: Chemistry ; Industrial Chemistry and Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Particles comparable in size to or larger than the measurement volume need extra consideration when measured by a phase-Doppler system. The phase of the Doppler burst received when such particles traverse the measurement volume depends not only on the size of the particle but also on its trajectory, since the particle is not uniformly illuminated. This paper presents a strategy for securing correct measurements even under such conditions, taking advantage of the three-detector receiving optics of the Dantec Particle Dynamics Analyzer. The effectiveness of the approach is demonstrated for sizing drops in liquid-gas and liquid-liquid two-phase flows: water drops in air, water drops in FC72 and FC72 drops in water. The combination of water and FC72 is also of interest because the relative refractive index is close to unity. Measurements of drops size were made on a monodisperse stream of drops about 2 mm in diameter, i.e. substantially larger than the measurement volume, and polydisperse distributions of drops ranging in diameter from below 0.2 mm to about 1 mm.
    Additional Material: 20 Ill.
    Type of Medium: Electronic Resource
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