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  • Articles  (108)
  • 1990-1994  (108)
  • Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics  (108)
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  • Articles  (108)
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  • 1
    Electronic Resource
    Electronic Resource
    Positive temperature coefficient of resistance effect in hot-pressed cristobalite-silicon carbide composites (1994)
    Springer
    Journal of materials science 29 (1994), S. 1097-1100 
    Details
    ISSN: 1573-4803
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Abstract Conductive silicon carbide particles were incorporated into an insulating cristobalite ceramic matrix to produce composite materials with a sizeable positive temperature coefficient (PTC) effect. A large drop in resistivity with silicon carbide content at room temperature, or percolation behaviour, was observed. The PTC effect of the composites, which resulted from the thermal expansion of the cristobalite ceramic matrix, was a maximum with five orders of magnitude for the specimen with 25 vol% silicon carbide. The PTC transition temperature of the composites was at 260 °C, which coincided exactly the reversible high-low phase inversion temperature of the cristobalite ceramic matrix.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00351437
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  • 2
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    Positive temperature coefficient of resistance effect in hot-pressed cristobalite-silicon carbide composites (1994)
    Springer
    Details
    Publication Date: 1994-02-01
    Print ISSN: 0022-2461
    Electronic ISSN: 1573-4803
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Published by Springer
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    PAPER CURRENT
  • 3
    Electronic Resource
    Electronic Resource
    Structure and chemistry of silicon nitride and silicon carbonitride thin films deposited from ethylsilazane in ammonia or hydrogen (1992)
    s.l. : American Chemical Society
    Chemistry of materials 4 (1992), S. 478-483 
    Details
    ISSN: 1520-5002
    Source: ACS Legacy Archives
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1021/cm00020a044
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  • 4
    Electronic Resource
    Electronic Resource
    FRACTURE BEHAVIOUR OF AXISYMMETRIC BARS UNDER HIGH TRIAXIAL STRESS AND LARGE STRAIN CYCLIC LOADING (1992)
    Oxford, UK : Blackwell Publishing Ltd
    Fatigue & fracture of engineering materials & structures 15 (1992), S. 0 
    Details
    ISSN: 1460-2695
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Axisymmetric notched bars with notch roots of large and small radius were tested under large strain cyclic loading. The main attention is focused on the fracture behaviour of steels having cycles to failure within the range 1-100. Our study shows that a gradual transition from a static ductile nature to one of fatigue cleavage can be observed and characterized by the Coffin-Manson formula in a generalized form. Both the triaxial tensile stress within the central region of specimens and static damage caused by the first increasing load have effects on the final failure event. A generalized cyclic strain range parameter δε is proposed as a measure of the numerous factors affecting behaviour. Fractographs are presented to illustrate the behaviour reported in the paper.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1111/j.1460-2695.1992.tb00028.x
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  • 5
    Electronic Resource
    Electronic Resource
    CRACK TIP BEHAVIOUR AND CRACK PROPAGATION IN DUCTILE MATERIALS (1992)
    Oxford, UK : Blackwell Publishing Ltd
    Fatigue & fracture of engineering materials & structures 15 (1992), S. 0 
    Details
    ISSN: 1460-2695
    Source: Blackwell Publishing Journal Backfiles 1879-2005
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Dilatational plastic equations, which can include the effects of ductile damage, are derived based on the equivalency in expressions for dissipated plastic work. Void damage developed internally at the large-strain stage is represented by an effective continuum being strain-softened and plastically dilated. Accumulation of this local damage leads to progressive failure in materials. With regard to this microstructural background, the constitutive parameters included for characterizing material behaviour have the sense of internal variables. They are not able to be determined explicitly by macroscopic testing but rather through computer simulation of experimental curves and data. Application of this constitutive model to mode-I cracking examples demonstrates that a huge strain concentration accompanied by a substantial drop of stress does occur near the crack tip. Eventually, crack propagation is simulated by using finite elements in computations. Two numerical examples show good accordance with experimental data. The whole procedure of study serves as a justification of the constitutive formulation proposed in the text.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1111/j.1460-2695.1992.tb00048.x
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  • 6
    Electronic Resource
    Electronic Resource
    Syntheses of polysilanes having cyclodisilazane units in the backbone (1992)
    Springer
    Polymer bulletin 27 (1992), S. 607-613 
    Details
    ISSN: 1436-2449
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Summary Polysilanes containing cyclodisilazane units in the backbone were synthesized by the modified Wurtz-type coupling of available dichlorosilanes with N,N′-bis (chlorodimethylsilyl)tetramethylcyclodisilazane in the mixture of solvents. The effect of solvent additives on the polymerization process was examined. These polymers are soluble in common solvents and very easily handled by molding or casting.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00297429
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  • 7
    Electronic Resource
    Electronic Resource
    Syntheses, crystal structures, and characterizations of two novel cubane-like and double cubane-like molybdenum-copper-sulphur clusters {MoCu3S3(S2COEt)}(O)(Ph3P)3 and {Mo2Cu6S6(SCMe3)2}(O)2(Ph3P)4 (1992)
    Springer
    Journal of cluster science 3 (1992), S. 201-218 
    Details
    ISSN: 1572-8862
    Keywords: Cubane-like ; double cubane-like ; Molybdenum-copper-sulphur clusters
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Two novel heterometallic cubane-like and double cubane-like clusters, {MoCu3S3(S2COEt)}(O)(Ph3P)3 I and {Mo2Cu6S6(SCMe3)2}(O)2(Ph3P)4 II, were synthesized by reaction of {MoCu2S3}(O)(Ph3P)3 with CuS2COEt and CuSCMe3, respectively. ClusterI crystallized in the triclinic space group $$P\overline 1 $$ (2) witha=12.766(6) Å,b=22.904(5) Å,c=10.522(3) Å, α=99.86(2)°, β=109.68(2)°, γ=86.84(3)°,V=2854(2) Å3,Z=2,R=0.049 for 6622 observed reflections (I〉5σ(I)) and 410 variables. ClusterII crystallized in the triclinic space group $$P\overline 1 $$ (2) with dimensionsa=14.212(4) Å,b=14.725(5) Å,c=12.396(8) Å, α=110.32(4)°, β=90.40(5)°, γ=62.88(2)°,V=2129(2) Å3,Z=1,R=0.039 for 6020 observed reflections (I〉3σ(I)) and 461 variables. ClusterI consists of a neutral cubane-like molecule with the core {MoCu3S3(S2COEt)}2+, in which one corner of the cubane-like core is a novel triply bridging bidentate 1,1-dithiolato (xanthate, S2COEt−) ligand. ClusterII is a double cubane-like one, in which two cubane-like cores {MoCu3S3(SCMe3)}2+ are connected by two Cu-S bonds of the triply bridging monothiolato (SCMe 3 − ) ligand. Two different pathways of unit construction from a small heterometallic cluster {MoCu2S3}(O)(Ph3P)3 have been outlined. Comparisons of the selected bond lengths and bond angles for the cubane-like core {MoCu3S3 X} (X=Cl−, Br−, S2COEt−, SCMe 3 − ) are given. Spectroscopic properties of the title clusters are also reported.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00702883
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  • 8
    Electronic Resource
    Electronic Resource
    The designed synthesis and crystallographic characterization of three novel heterotrimetallic linear complexes of [Et4N][(Ph3P)2{M′S2 MS2Fe}Cl2] (M=Mo,M′=Ag;M=W,M′=Cu, Ag) (1993)
    Springer
    Journal of cluster science 4 (1993), S. 89-103 
    Details
    ISSN: 1572-8862
    Keywords: Designed synthesis ; heterotrimetallic ; linear complexes
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The complexes [Et4N][(Ph3P)2{M′S2 MS2Fe}Cl2] (M=Mo,M′=Ag;M=W,M′=Cu, Ag) have been obtained by reaction of [Et4N]2[S2 MS2FeCl2] (M=Mo, W) with Cu(PPh3)3Cl or Ag(PPh3)3NO3 in MeCN/CH2Cl2, respectively. Crystal data for [Et4N][(PPh3)2 {AgS2MoS2Fe}Cl2] (I): triclinic, P $$\bar 1$$ (No. 2),Z=2,a=13.41(1)Å,b=15.54(1)Å,c=12.30(1)Å, α=105.24(6)°, β=94.63(7)°, γ=101.38(6)°, andV=2399(4)Å3. The bond lengths of Mo-Fe bond and the Mo-Ag distance are 2.756(2)Å and 3.033(2)Å, respectively. Crystal data for [Et4N][(PPh3)2 {AgS2WS2Fe}Cl2] (II): triclinic, P $$\bar 1$$ (No. 2),Z=2,a=13.457(5))Å,b=15.601(6)Å,c=12.338(4)Å, α=105.20(3)°, β=94.61(4)°, γ=101.43(4)°, andV=2426(2)Å3. The bond length of W-Fe bond and the W-Ag distance are 2.786(2)Å and 3.076(1)Å, respectively. Crystal data for [Et4N][(PPh3)2 {CuS2WS2Fe}Cl2] (III): triclinic, P $$\bar 1$$ (No. 2),Z=2,a=13.498(5)Å,b=15.372(4)Å,c=12.340(4)Å, α=105.54(2)°, β=93.32(3)°, γ=101.40(3)°, andV=2401(1)Å3. The bond lengths of W-Fe bond and the W-Cu bond are 2.800(1)Å and 2.851(1)Å, respectively.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00702711
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  • 9
    Electronic Resource
    Electronic Resource
    Designed synthesis for some transition metal clusters involving bridging-sulfido ligand (1994)
    Springer
    Journal of cluster science 5 (1994), S. 265-285 
    Details
    ISSN: 1572-8862
    Keywords: Designed synthesis ; transition metal clusters
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract Designed synthesis for some transition metal clusters involving bridging-sulfido ligands is reviewed. The basic concept with the use of reactive fragments as building blocks is described. It is shown that the sulfido ligands with lone-pair electrons and the unsaturated coordination sites play important roles in this rational synthesis. The relationship between the metallic coordination types of the sulfido ligands and their assembling activity in the compounds is summarized. Examples of the six kinds of “unit construction” with reactive fragments as building blocks are shown, indicating clearly that the “unit construction” is a reasonable way in the synthesis of transition metal clusters involving bridging sulfido ligands. Finally, the potential application of the “unit construction” schemes in the synthesis of transition metal clusters involving other bridging ligands is presented.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01170712
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  • 10
    Electronic Resource
    Electronic Resource
    Determination of Energy Level of Atomic H in Crystalline Silicon by Use of Hydrogenation of Radiation Defects (1991)
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 38-41 (Jan. 1991), p. 1021-1026 
    Details
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Type of Medium: Electronic Resource
    URL: http://www.tib-hannover.de/fulltexts/2011/0528/02/05/transtech_doi~10.4028%252Fwww.scientific.net%252FMSF.38-41.1021.pdf
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