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  • INORGANIC AND PHYSICAL CHEMISTRY  (2)
  • YBCO  (1)
  • 1990-1994  (3)
  • 1
    Electronic Resource
    Electronic Resource
    Microstructures of high-J c melt-textured YBa2Cu3O7−x /Ag superconductors (1994)
    Springer
    Journal of superconductivity 7 (1994), S. 947-950 
    Details
    ISSN: 1572-9605
    Keywords: Critical current density ; Ag addition ; grain alignment ; flux pinning ; defect structure ; YBCO ; melt-texturing
    Source: Springer Online Journal Archives 1860-2000
    Topics: Electrical Engineering, Measurement and Control Technology , Physics
    Notes: Abstract Silver has been previously added to the melt-textured YBa2Cu3O7−x in order to increase the critical current density (J c ) of these materials. However, the effect of this addition on theJ c is presently unclear. The purpose of this study is to investigate the effect of silver on both critical current density and the microstructure of the melt-textured YBa2Cu3O7−x superconductors by means of X-ray diffraction, optical polarized microscopy, and transmission electron microscopy (TEM). TheJ c of the MTG YBCO/Ag samples is more than 104A/cm2 under the 5 kOe magnetic field. It has been shown that as the concentration of silver increases, the fraction of the 211 phase dispersed within the 123 matrix decreases. Therefore, theJ c slightly decreases. These results, together with the effect of the 211 phase, dislocations, and other structure defects on flux pinning, are described in this paper.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF00732277
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    Paper (German National Licenses)
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  • 2
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    Production of oxygen from lunar ilmenite (1991)
    In:  CASI
    Details
    Publication Date: 2013-08-31
    Description: The kinetics and the mechanism of reduction of synthetic ilmenite by hydrogen in the temperature range of 807 to 1014 C were investigated. At temperatures below 876 C, the temporal profiles of conversion have a sigmoidal shape and indicate the presence of three different stages (induction, acceleration, and deceleration) during the reduction reaction. The apparent activation energy for the reaction is 22.3 kcal/mole, whereas the intrinsic activation energy is 16.9 kcal/mole. Scanning electron microscopy and energy dispersive x-ray analyses show that the diffusion of Fe product away from the reaction front and through the TiO2 phase, followed by the nucleation and growth of a separate Fe phase is an important step affecting the process kinetics. X-ray diffraction and wavelength dispersive x-ray results indicate that the TiO2 can be reduced to lower oxides of titanium at temperatures higher than 876 C.
    Keywords: INORGANIC AND PHYSICAL CHEMISTRY
    Type: NASA Space Engineering Research Center for Utilization of Local Planetary Resources; 29 p
    Format: application/pdf
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    NASA TECHNICAL REPORTS
  • 3
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    Production of oxygen from lunar ilmenite (1990)
    In:  CASI
    Details
    Publication Date: 2013-08-31
    Description: The following subjects are addressed: (1) the mechanism and kinetics of carbothermal reduction of simulated lunar ilmenite using carbon and, particularly, CO as reducing agents; (2) the determination of the rate-limiting steps; (3) the investigation of the effect of impurities, particularly magnesium; (4) the search for catalysts suitable for enhancement of the rate-limiting step; (5) the comparison of the kinetics of carbothermal reduction with those of hydrogen reduction; (6) the study of the combined use of CO and hydrogen as products of gasification of carbonaceous solids; (7) the development of reduction methods based on the use of waste carbonaceous compounds for the process; (8) the development of a carbothermal reaction path that utilizes gasification of carbonaceous solids to reducing gaseous species (hydrocarbons and carbon monoxide) to facilitate the reduction reaction kinetics and make the process more flexible in using various forms of carbonaceous feeds; (9) the development of advanced gas separation techniques, including the use of high-temperature ceramic membranes; (10) the development of an optimum process flow sheet for carbothermal reduction, and comparison of this process with the hydrogen reduction scheme, as well as a general comparison with other leading oxygen production schemes; and (11) the use of new and advanced material processing and separation techniques.
    Keywords: INORGANIC AND PHYSICAL CHEMISTRY
    Type: NASA Space Engineering Research Center for Utilization of Local Planetary Resources; 5 p
    Format: application/pdf
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    NASA TECHNICAL REPORTS
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