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  • 1
    Electronic Resource
    Electronic Resource
    The determination of the isotacticity of polypropylene in the 90-100% range by infrared spectroscopyPresented as a paper before the Meeting of the American Chemical Society Division of Polymer Chemistry, September 1963, in New York City. At that time this laboratory was the Research Center of the Spencer Chemical Company. (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 417-425 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: An infrared method has been developed for the determination of the isotacticity of polypropylene in the 90-100% range. The method requires the annealing of thin films at 165-167°C. for 3 hr. in an inert atmosphere, followed by slow cooling to room temperature. For approximate answers the ratio of the intensity of the 10.00 μ band to that of the 10.27 μ band can be reported as the fraction of isotactic material. Better results are obtained, however, by using Figure 2 as a calibration curve and reading the values from it.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070130302
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  • 2
    Electronic Resource
    Electronic Resource
    PBI powder processing to performance parts (1994)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 53 (1994), S. 485-496 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: A new route (“direct forming”) was developed for forming dense PBI shapes from PBI powder. The new process affords the possibility of automated PBI powder shaping (“cold compaction”) and densification in batches of multiple parts by a “powder-assisted hot isostatic pressing” process. Direct forming is a more productive alternative to hot compression molding. Two developments enable PBI direct forming: (1) the discovery that PBI powders that are porous and plasticized with moisture can be shaped by compaction at ambient temperatures (cold-compacted), and (2) a finding that cold-compacted shapes can be densified in large batches by a powder-assisted hot isostatic pressing. The porous PBI powder is formed from PBI in solution by a spray-precipitation process. When plasticized with moisture, this powder is cold-compactible to PBI shapes with densities up to 94% of that of ultimate density of PBI. These shapes, which have sufficient strength to be handled, are then further consolidated via powder-assisted hot isostatic pressing to shapes with excellent thermal and mechanical properties and densities of about 99% of the ultimate. © 1994 John Wiley & Sons, Inc.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1994.070530503
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  • 3
    Electronic Resource
    Electronic Resource
    Effect of type and amount of comonomer on the properties of four copolymers of ethylene (1966)
    Stamford, Conn. [u.a.] : Wiley-Blackwell
    Polymer Engineering and Science 6 (1966), S. 5-14 
    Details
    ISSN: 0032-3888
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The plastics industry is now coming to realize that copolymers are unique thermoplastics which have broad areas of application. It is believed that ethylene-methyl acrylate copolymers of 2 melt index may be extrusion coated to paper by a cap-coat process or by use of a chill roll with an adhesive coating. Copolymers of ethylene and vinyl monomers can be made into film by the same methods used for polyethylene. Methyl acrylate and methyl methacrylate copolymers may be processed on a wide range of molding equipment. Table VII in the article gives a list of applications for each polymer, along with expected physical properties.
    Additional Material: 16 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pen.760060103
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  • 4
    Electronic Resource
    Electronic Resource
    Fast-atom bombardment/mass-analysed ion kinetic energy spectrometry of inositol phosphates (1993)
    New York, NY : Wiley-Blackwell
    Rapid Communications in Mass Spectrometry 7 (1993), S. 555-560 
    Details
    ISSN: 0951-4198
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The application of fast-atom bombardment mass Spectrometry and collisiorutlly induced dissociation with mass-analysed ion kinetic energy (CID/MIKE) Spectrometry of representative inositol mono-, bis- and trisphos-phates is described. Based on their CID/MIKE spectra, inositol polyphosphates containing vicinal phosphate groups could be distinguished from isomers in which adjacent phosphate groups were absent. The potential value of this procedure in studies of the biochemistry of intracellular second messengers is discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/rcm.1290070631
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  • 5
    Electronic Resource
    Electronic Resource
    Transparent barrier resins with high nitrile content (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 2567-2577 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The effect of 30-49 wt-% nitrile group content on the properties of copolymers is demonstrated. The nitrile is furnished by either acrylonitrile or methacrylonitrile. The exceptional resistance of such high nitrile content resins to the passage of gases and of solvents is shown and variations therein demonstrated for different comonomers. Transparent, tough, grafted polymers of good color are described which retain these properties. These qualities, combined with low second-order transition temperatures and adequate heat deflection temperatures, provide polymers of interest wherever containment and barrier are desired. Bottles, thermoformed containers, etc., could benefit from the use of some of the polymers described.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070131205
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  • 6
    Electronic Resource
    Electronic Resource
    Use of gas-liquid chromatography in the analysis of rigid polyurethane foam polyols (1969)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 13 (1969), S. 1297-1307 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Detailed characterization of the low molecular weight polyols used as intermediates in rigid polyurethane foam production has not been feasible to date. Gas-liquid chromatography of the trimethylsilyl ether derivatives of the polyols now offers a more complete picture of polyol composition, particularly with regard to the molecular weight distribution. The data may be interpreted on a semiquantitative basis. The study of processing variables in polyol manufacture, detection of impurities and analysis of unknown polyols or those based on mixed initiators may all be facilitated by use of this GLC technique.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1969.070130617
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  • 7
    Electronic Resource
    Electronic Resource
    Characterization of glucuronic acid conjugates of a novel angiotensin receptor antagonist (1994)
    New York, NY : Wiley-Blackwell
    Rapid Communications in Mass Spectrometry 8 (1994), S. 217-221 
    Details
    ISSN: 0951-4198
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Nanogram quantities of glucuronic acid conjugates of GR117289 in rat and dog bile have been analysed by semi-microbore high-performance liquid chromatography (HPLC)/ionspray mass spectrometry with on-line UV diode array detection. The determination of drug metabolites in bile has often proved problematical due to the large number of endogenous components in this biological matrix, in particular the bile acids. Semi-microbore HPLC is useful for concentrating small quantities of material and, in combination with an on-line diode array detector, for distinguishing between drug related and endogenous components. A novel angiotensin II receptor antagonist, GR117289, had proved difficult to analyse by thermospray mass spectrometry because of its thermal lability. The use of the less thermally dependent technique of ionspray mass spectrometry allowed the characterization of nanogram quantities of glucuronic acid metabolites of GR117289 in bile.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/rcm.1290080218
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  • 8
    Electronic Resource
    Electronic Resource
    Poly-α-cyanostyrene (1965)
    New York : Wiley-Blackwell
    Journal of Polymer Science Part A: General Papers 3 (1965), S. 1527-1533 
    Details
    ISSN: 0449-2951
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The monomer α-cyanostyrene polymerized at a very slow rate under the influence of free-radical initiators. Rapid polymerization to high molecular weight material was achieved by using anionic initiators (tri-n-butylphosphine and tetrakisdimethylaminotitanium). The polymer made at -78°C. was colorless, fusible, soluble, and had a number-average molecular weight of over 5,000. The polymer prepared at 0°C. was brown, insoluble, and infusible. None of the polymer showed order in the x-ray diagram. The rate of dimerization of α-cyanostyrene under a wide variety of conditions was measured. Two new derivatives of the intermediate, 3-(N,N-dimethylamino)-2-phenylpropionitrile were prepared: the methiodide, m.p. 242-245°C. (decomp.), and the picrate, m.p. 116.5-117.5°C.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/pol.1965.100030420
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