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  • On-column injection
  • Wiley-Blackwell  (4)
  • American Geophysical Union
  • Nature Publishing Group
  • Oxford University Press
  • Springer Nature
  • 1990-1994  (1)
  • 1980-1984  (3)
Sammlung
Schlagwörter
Verlag/Herausgeber
  • Wiley-Blackwell  (4)
  • American Geophysical Union
  • Nature Publishing Group
  • Oxford University Press
  • Springer Nature
Erscheinungszeitraum
  • 1990-1994  (1)
  • 1980-1984  (3)
Jahr
  • 1
    Digitale Medien
    Digitale Medien
    High temperature (GC)2 and (GC)2/CI-MS of nucleosides: Analysis of purinyl nucleoside isomer composition (1980)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 3 (1980), S. 161-165 
    Details
    ISSN: 0935-6304
    Schlagwort(e): GC, GC/MS ; Capillary, HMDS-deactivated ; On-column injection ; Nucleoside linkage isomers ; Separation, structural assignment feasibilities ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: The analysis of low-volatile polar nucleosides by (GC)2/FID and (GC)2/CI-MS, employing HMDS-deactivated glass capillary columns and on-column injection, is described. The four linkage isomers of a specific nucleoside, formed in the synthetic procedure, are in each case sufficiently well separated in the chromatogram; GC/CI-MS allows for a differentiation of N-7 and N-9 linkage isomers.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/jhrc.1240030402
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  • 2
    Digitale Medien
    Digitale Medien
    GC/MS analysis of chlorinated paraffins with negative ion chemical ionization (1984)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 33-37 
    Details
    ISSN: 0935-6304
    Schlagwort(e): Chlorinated paraffins ; Gas chromatography ; Mass spectrometry ; Negative ion ; Chemical ionization ; Capillary column ; On-column injection ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Although chlorinated paraffins (CP) are produced in large amounts (300 000 tonnes per year), little is known about their occurrence in the environment due to the lack of specific and sensitive analytical methods. The present paper describes the GC/MS analysis of different CP's using capillary gas chromatography with on-column injection and negative ion chemical ionization (NCI) mass spectrometry. Chromatographic resolution of groups of isomers and homologues was obtained. The chromatograms and mass spectra are discussed. The suitability of this method for trace analysis of a CP sample using multiple ion detection (MID) is described.
    Zusätzliches Material: 3 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/jhrc.1240070106
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  • 3
    Digitale Medien
    Digitale Medien
    Thermal degradation observed with different injection techniques: Quantitative estimation by the use of thermolabile carbamate pesticides (1990)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 13 (1990), S. 759-763 
    Details
    ISSN: 0935-6304
    Schlagwort(e): Thermal degradation ; N-methylcarbamate pesticides ; PTV injection ; On-column injection ; Splitless injection ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: An experiment has been designed to study the thermal degradation of thermolabile compounds caused by various injection techniques. The four carbamate pesticides aminocarb, bendiocarb, carbaryl, and dioxacarb decompose thermally into methylisocyanate and the corresponding phenol. The carbamets and the phenols arising from them were separated on a 25 m SE-54 fused silica column; all compounds exhibited sharp peak shape indicating that the degradation observed took place completely within the injector.When cold on-column injection was employed no thermal degradation was observed whereas with hot splitless injection at 220°C decomposition of the carbamates was almost complete.PTV injection was found to produce intermediate results. When packed with glass wool and operated with glass wool and operated with starting temperatures lower than the boiling point of the solvent, decomposition was found to be almost complete. Applying isothermal conditions at 140°C (30°C above the boiling point of toluene) aminocarb and bendiocarb underwent only slight decomposition while carbaryl and dioxacarb were about half degraded. Results from PTV injection with an empty insert resembled those obtained using cold on-column injection and in this mode the application of temperatures up to 200°C resulted in no visible degradation. This can be explained by the short residence time of the sample in the injector.
    Zusätzliches Material: 4 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/jhrc.1240131107
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  • 4
    Digitale Medien
    Digitale Medien
    Selective and non-selective sampling from precolumn separations - with emphasis on the sampling of aqueous solutionsPaper based on a poster presented at the Fifth International Symposium on Capillary Chromatography, Riva del Garda, Italy, April 26-28, 1983. (1984)
    Weinheim : Wiley-Blackwell
    Journal of High Resolution Chromatography 7 (1984), S. 4-12 
    Details
    ISSN: 0935-6304
    Schlagwort(e): Gas chromatography ; Immobilized capillary columns ; Aqueous solutions ; On-column injection ; Split injection ; Multidimensional separations ; Chemistry ; Analytical Chemistry and Spectroscopy
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Chemie und Pharmazie
    Notizen: Various methods of gas chromatographic analysis at high resolution and low detection limits in aqueous solutions are described with regard to sampling techniques, column technology, and the application of coupled pre-columns, also including multidimensional methods. Immobilized polyethylene glycol (Carbowax 20 M) columns have also been produced and used successfully.
    Zusätzliches Material: 11 Ill.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1002/jhrc.1240070102
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