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  • GEOPHYSICS  (12)
  • Analytical Chemistry and Spectroscopy  (5)
  • Astronomy
  • FLUID MECHANICS AND HEAT TRANSFER
  • ddc:330
  • 1990-1994  (19)
Collection
Keywords
Publisher
Years
Year
  • 1
    Electronic Resource
    Electronic Resource
    Molecular fragmentation patterns of carbon dioxide at very high internal energies (1993)
    Chichester : Wiley-Blackwell
    Biological Mass Spectrometry 28 (1993), S. 340-343 
    Details
    ISSN: 0030-493X
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Ion-ion coincidence measurements following K-shell absorption in the carbon dioxide molecule were performed by applying time-of-flight mass spectrometry in conjunction with monochromatic synchrotron radiation and electron impact. Identification of particularly sensitive electronic transitions and the consecutive molecular fragmentation in real time was performed. Analysis of coincidence recordings from decomposition of carbon dioxide reveals one distinct pathway in which three cations are formed following excitation of oxygen Is electrons.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/oms.1210280413
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    Paper (German National Licenses)
    Fulltext
  • 2
    Electronic Resource
    Electronic Resource
    Fast-atom bombardment/mass-analysed ion kinetic energy spectrometry of inositol phosphates (1993)
    New York, NY : Wiley-Blackwell
    Rapid Communications in Mass Spectrometry 7 (1993), S. 555-560 
    Details
    ISSN: 0951-4198
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: The application of fast-atom bombardment mass Spectrometry and collisiorutlly induced dissociation with mass-analysed ion kinetic energy (CID/MIKE) Spectrometry of representative inositol mono-, bis- and trisphos-phates is described. Based on their CID/MIKE spectra, inositol polyphosphates containing vicinal phosphate groups could be distinguished from isomers in which adjacent phosphate groups were absent. The potential value of this procedure in studies of the biochemistry of intracellular second messengers is discussed.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/rcm.1290070631
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    Paper (German National Licenses)
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  • 3
    Electronic Resource
    Electronic Resource
    Characterization of glucuronic acid conjugates of a novel angiotensin receptor antagonist (1994)
    New York, NY : Wiley-Blackwell
    Rapid Communications in Mass Spectrometry 8 (1994), S. 217-221 
    Details
    ISSN: 0951-4198
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: Nanogram quantities of glucuronic acid conjugates of GR117289 in rat and dog bile have been analysed by semi-microbore high-performance liquid chromatography (HPLC)/ionspray mass spectrometry with on-line UV diode array detection. The determination of drug metabolites in bile has often proved problematical due to the large number of endogenous components in this biological matrix, in particular the bile acids. Semi-microbore HPLC is useful for concentrating small quantities of material and, in combination with an on-line diode array detector, for distinguishing between drug related and endogenous components. A novel angiotensin II receptor antagonist, GR117289, had proved difficult to analyse by thermospray mass spectrometry because of its thermal lability. The use of the less thermally dependent technique of ionspray mass spectrometry allowed the characterization of nanogram quantities of glucuronic acid metabolites of GR117289 in bile.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/rcm.1290080218
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    Paper (German National Licenses)
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  • 4
    Electronic Resource
    Electronic Resource
    Structures of zearalenone and zearalanone in solution: A high-field NMR and molecular modelling study (1990)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 28 (1990), S. 835-845 
    Details
    ISSN: 0749-1581
    Keywords: Zearalenone ; Zearalanone ; 1H and 13C NMR ; Molecular modelling ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The complete 1H and 13C NMR spectra of the mycotoxin zearalenone are described. An analysis of all the vicinal proton-proton coupling constants, together with molecular modelling results, leads to a three-dimensional structure very similar to those observed x-ray crystallographically for related systems. Analogous data on zearalanone reveal that whereas the overall molecular geometry is similar to that of zearalenone, the alkyl terminus of the 12-membered bridging moiety is now oriented almost orthogonally to the aromatic ring plane.
    Additional Material: 10 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260281002
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    Paper (German National Licenses)
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  • 5
    Electronic Resource
    Electronic Resource
    NMR analysis of fluorinated corticosteroids related to fluocinonide: Detection of long-range 1H-19F couplings using the heteronuclear equivalent of the COSY experiment (1991)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 29 (1991), S. 387-397 
    Details
    ISSN: 0749-1581
    Keywords: 1H NMR ; 19F Corticosteroids ; 1H-19F long-range coupling ; Heteronuclear COSY ; 1H-19F 2D correlation ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The analysis of the 1H and 19F NMR spectra of the corticosteroid fluocinonide and five related steroids is reported. The 500 MHz 1H NMR spectra revealed several previously undetected long-range 1H-19F coupling constants. These couplings were assigned by the application of the heteronuclear equivalent of the COSY pulse sequence. The fluorine substituent effects and long-range heteronuclear couplings were examined in relation to structures derived from molecular mechanics (MMX) calculations.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260290417
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  • 6
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    Dayside ionospheric convection changes in response to long-period interplanetary magnetic field oscillations - Determination of the ionospheric phase velocity (1992)
    In:  Other Sources
    Details
    Publication Date: 2011-08-24
    Description: Ground magnetic field perturbations recorded by the CANOPUS magnetometer network in the 7 to 13 MLT sector are used to examine how reconfigurations of the dayside polar ionospheric flow take place in response to north-south changes of the IMF. During the 6-h interval in question, IMF Bz oscillates between +/- 7 nT with about a 1-h period. Corresponding variations in the ground magnetic disturbance are observed which we infer are due to changes in ionospheric flow. Cross correlation of the data obtained from two ground stations at 73.5 deg magnetic latitude, but separated by about 2 hours in MLT, shows that changes in the flow are initiated in the prenoon sector (about 10 MLT) and then spread outward toward dawn and dusk with a phase speed of about 5 km/s over the longitude range about 8 to 12 MLT, slowing to about 2 km/s outside this range. Cross correlating the data from these ground stations with IMP 8 IMF Bz records produces a MLT variation in the ground response delay relative to the IMF which is compatible with these deduced phase speeds.
    Keywords: GEOPHYSICS
    Type: Journal of Geophysical Research (ISSN 0148-0227); 97; A12; p. 19,373-19,380.
    Format: text
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    NASA TECHNICAL REPORTS
  • 7
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    Hubble Space Telescope First Observations of the Brightest Stars in the Virgo Galaxy M100 = NGC 4321 (1994)
    In:  Other Sources
    Details
    Publication Date: 2018-06-08
    Description: As part of both the Early Release Observations fromthe Hubble Space Telescope and the Key PRoject on the Extragalctic Distance Scale, we have obtained multi-wavelength BVR WFPC2 images for the face-on Virgo cluster spiral galaxy M11 = NGC 4321.
    Keywords: Astronomy
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  • 8
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    Observations of Earthward and tailward propagating flux rope plasmoids: Expanding the plasmoid model of geomagnetic substorms (1994)
    In:  Other Sources
    Details
    Publication Date: 2019-07-13
    Description: A survey of Interplanetary Monitoring Platform (IMP 8) magnetometer data for plasmoid signatures during magnetospheric intervals from 1981 through 1983 found 16 plasmoids and 37 traveling compression regions as well as two earthward propagating flux ropes and 19 south-north bipolar lobe signatures. The properties of these relatively near-Earth plasmoids, traveling compression regions, and earthward propagating flux ropes and a qualitative model for their formation are presented. The plasmoids have estimated sizes, durations, magnetic field signatures, downtail velocities, and substorm associations very similar to those of the plasmoids identified in International Sun-Earth Explorer (ISEE) 3 deep-tail observations. The occurrence frequency of these near-Earth plasma sheet plasmoids is significantly smaller than that of plasmoids found in the mid- and deep tail with ISEE 3. The earthward propagating flux ropes are characterized by a south-north bipolar turning in the Geocentric Solar Magnetospheric (GSM) B(sub z) component, are localized near the noon-midnight meridional plane, and are strongly correlated with interplanetary magnetic field B(sub z) north and small isolated high latitude geomagnetic substorms. These events are also apparently very rare and/or spatially localized. We propose that these structures are 'proto-plasmoids,' i.e., plasmoids for which near-Earth magnetic reconnection stopped before all the closed plasma sheet field lines were reconnected. The proto-plasmoids are then 'trapped' inside closed magnetic field lines and propagate earthward owing to the effect of the distant X-line's earthward plasma flow. We suggest that the two different 'types' of plasmoids are due to the different energy states of the magnetosphere during periods of southward and northward interplanetary magnetic field.
    Keywords: GEOPHYSICS
    Type: Journal of Geophysical Research (ISSN 0148-0227); 99; A1; p. 183-198
    Format: text
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    NASA TECHNICAL REPORTS
  • 9
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    A globally convergent matrix-free algorithm for implicit time-marching schemes arising in finite element analysis in fluids (1991)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: A solution procedure for solving nonlinear time-marching problems is presented. The nonsymmetric systems of equations arising from a Newton-type linearization of these time-marching problems are solved using an iterative strategy based on the generalized minimal residual (GMRES) algorithm. Matrix-free techniques leading to reduction in storage are presented. Incorporation of a linesearch algorithm in the Newton-GMRES scheme is discussed. An automatic time-increment control strategy is developed to increase the stability of the time-marching process. High-speed flow computations demonstrate the effectiveness of these algorithms.
    Keywords: FLUID MECHANICS AND HEAT TRANSFER
    Type: Computer Methods in Applied Mechanics and Engineering (ISSN 0045-7825); 87; 3-Feb; 281-304
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    NASA TECHNICAL REPORTS
  • 10
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    Small-scale electrodynamics of the cusp with northward interplanetary magnetic field (1992)
    In:  Other Sources
    Details
    Publication Date: 2019-07-12
    Description: Possible low-altitude field signatures of merging occurring at high latitudes during a period of strong northward directed interplanetary magnetic field are reported. Large electric and magnetic field spikes detected at the poleward edge of the magnetosheathlike particle precipitation are interpreted as field signatures of the low-altitude footprint of such merging line locations. A train of phase-shifted, almost linearly polarized electric and magnetic field fluctuations was detected just equatorward of the large electromagnetic spike. It is argued that these may be due to either ion cyclotron waves excited by penetrating magnetosheath ions or transient oscillations in the frame of convecting plasma, brought about by the sudden change in the flow at the magnetospheric end of the field line.
    Keywords: GEOPHYSICS
    Type: Journal of Geophysical Research (ISSN 0148-0227); 97; A5 M
    Format: text
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