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  • 1995-1999  (2)
  • 1
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 32 (1999), S. 442-451 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: A monochromatic Laue technique is used to extract information about the reciprocal lattice of a quasicrystal. A synchrotron beamline, normally available for protein crystallography, was used in this study. Each photograph is a planar projection of a spherical cap, a portion of the Ewald sphere, in reciprocal space. The algorithms needed to relate the images to reciprocal space are described in detail. It is found that many weak, but readily detectable, Bragg reflections are found in unexpected positions in reciprocal space, as predicted from theory. Some very weak Bragg reflections are clearly visible on the imaging plate, but could not be detected by photon counting using a four-circle diffractometer. Some images show characteristic `rings' or `arcs' of diffuse scattering, as previously observed in other icosahedral quasicrystals. In view of the `extreme perfection' of the quasicrystalline specimen used in this study, it is proposed to view these rings (or arcs) as intrinsic features of the icosahedral quasicrystalline structure.
    Type of Medium: Electronic Resource
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  • 2
    Publication Date: 1999-06-01
    Description: A monochromatic Laue technique is used to extract information about the reciprocal lattice of a quasicrystal. A synchrotron beamline, normally available for protein crystallography, was used in this study. Each photograph is a planar projection of a spherical cap, a portion of the Ewald sphere, in reciprocal space. The algorithms needed to relate the images to reciprocal space are described in detail. It is found that many weak, but readily detectable, Bragg reflections are found in unexpected positions in reciprocal space, as predicted from theory. Some very weak Bragg reflections are clearly visible on the imaging plate, but could not be detected by photon counting using a four-circle diffractometer. Some images show characteristic `rings' or `arcs' of diffuse scattering, as previously observed in other icosahedral quasicrystals. In view of the `extreme perfection' of the quasicrystalline specimen used in this study, it is proposed to view these rings (or arcs) as intrinsic features of the icosahedral quasicrystalline structure.
    Print ISSN: 0021-8898
    Electronic ISSN: 1600-5767
    Topics: Geosciences , Physics
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