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  • (iso-branched) C17 sphingoid-bases  (1)
  • Keywords. Ti-stabilized steels; soft-X-ray spectrometry; LEEIXS  (1)
  • 06A15
  • Springer  (2)
  • 1995-1999  (2)
Collection
Keywords
Publisher
  • Springer  (2)
Years
Year
  • 1
    Electronic Resource
    Electronic Resource
    Characterization of Precipitates in Ti-Stabilized Steels with Low-Energy Electron-Induced X-Ray Spectrometry and Scanning Electron Microscopy (1999)
    Springer
    Microchimica acta 131 (1999), S. 191-197 
    Details
    ISSN: 1436-5073
    Keywords: Keywords. Ti-stabilized steels; soft-X-ray spectrometry; LEEIXS ; XRF ; SEM.
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract  Various kinds of precipitates can influence the mechanical properties of Ti-stabilized steels. The qualitative composition of the Ti inclusions can be characterized microscopically, whereas for quantitative information to be obtained time-consuming selective dissolution must be used. The present study aims at chemical speciation of the isolated precipitates as a solid phase with the help of soft-X-ray spectrometry. Whether the method is capable of giving both qualitative and quantitative information on the composition of Ti-mixtures is discussed. The precipitates in Ti-stabilized steels are investigated after chemical dissolution of the steel matrix with a bromine/methanol mixture (1:10). By combination of soft-X-ray spectrometry with X-ray fluorescence (XRF) and scanning electron microscopy (SEM) both qualitative and quantitative characterization of the precipitates can be performed. They were found to consist mainly of TiC and TiN.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/PL00010033
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  • 2
    Electronic Resource
    Electronic Resource
    Structural analysis of neutral glycosphingolipids from Ascaris suum adults (Nematoda: Ascaridida) (1997)
    Springer
    Glycoconjugate journal 14 (1997), S. 389-399 
    Details
    ISSN: 1573-4986
    Keywords: arthro-series glycosphingolipids ; Ascaris suum ; (iso-branched) C17 sphingoid-bases ; neutral glycosphingolipids ; parasitic nematodes
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract The neutral glycosphingolipid fraction from adults of the pig parasitic nematode, Ascaris suum, was resolved into four components on thin-layer chromatography. The high-performance liquid chromatography-isolated components were structurally analysed by: methylation analysis; exoglycosidase cleavage; gas-liquid chromatography/mass spectrometry; liquid secondary-ion mass spectrometry; and, in particular, matrix-assisted laser desorption/ionization time-of-flight mass spectrometry. Their chemical structures were determined as: Glc(β1-1)ceramide, Man(β1-4)Glc(β1-1)ceramide, GlcNAc(β1-3)Man(β1-4)Glc(β1-1)ceramide and Gal(α1-3)GalNAc(β1-4)GlcNAc(β1-3)Man(β1-4)Glc(β1-1)ceramide; and were characterized as belonging to the arthro-series of protostomial glycosphingolipids. No glycosphingolipid component corresponding to ceramide tetrasaccharide was detected during these analyses. The ceramide composition of the parent glycosphingolipids was dominated by the 2-(R)-hydroxy C24:0 fatty acid, cerebronic acid, and C17 sphingoid-bases: 15-methylhexadecasphing-4-enine and 15-methylhexadecaphinganine in approximately equal proportions. The component ceramide monohexoside was characterized by an additional 15-methylhexadecaphytosphingosine. Abbreviations: CDH, ceramide dihexoside; Cer, ceramide; CMH, ceramide monohexoside; CPH, ceramide pentahexoside; CTH, ceramide trihexoside; CTetH, ceramide tetrahexoside; Hex, hexose; HexNAc, N-acetylhexosamine; HPTLC, high-performance thin-layer chromatography; LSIMS, liquid secondary-ion mass spectrometry; MALDI-TOF-MS, matrix-assisted laser desorption/ionization time-of-flight mass spectrometry; N-, Nz- and A-glyco(sphingo)lipids, neutral, neutralzwitterionic and acidic glyco(sphingo)lipids, respectively
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1018530914067
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