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  • 1
    Call number: 11/M 03.0009
    In: Reviews in mineralogy & geochemistry
    Description / Table of Contents: This volume was produced in response to the need for a comprehensive introduction to the continually evolving state of the art of synchrotron radiation applications in low-temperature geochemistry and environmental science. It owes much to the hard work and imagination of the devoted cadre of sleep-deprived individuals who blazed a trail that many others are beginning to follow. Synchrotron radiation methods have opened new scientific vistas in the earth and environmental sciences, and progress in this direction will undoubtedly continue. The organization of this volume is as follows. Chapter 1 (Brown and Sturchio) gives a fairly comprehensive overview of synchrotron radiation applications in low temperature geochemistry and environmental science. The presentation is organized by synchrotron methods and scientific issues. It also has an extensive reference list that should prove valuable as a starting point for further research. Chapter 2 (Sham and Rivers) describes the ways that synchrotron radiation is generated, including a history of synchrotrons and a discussion of aspects of synchrotron radiation that are important to the experimentalist. The remaining chapters of the volume are organized into two groups. Chapters 3 through 6 describe specific synchrotron methods that are most useful for single-crystal surface and mineral-fluid interface studies. Chapters 7 through 9 describe methods that can be used more generally for investigating complex polyphase fine-grained or amorphous materials, including soils, rocks, and organic matter. Chapter 2 (Shearer) reviews the behavior of Be in the Solar System, with an emphasis on meteorites, the Moon and Mars, and the implications of this behavior for the evolution of the solar system. Chapter 3 (Ryan) is an overview of the terrestrial geochemistry of Be, and Chapter 7 (Vesely, Norton, Skrivan, Majer, Kr·m, Navr·til, and Kaste) discusses the contamination of the environment by this anthropogenic toxin. Chapter 3 (Fenter) presents the elementary theory of synchrotron X-ray reflectivity along with examples of recent applications, with emphasis on in situ studies of mineral-fluid interfaces. Chapter 4 (Bedzyk and Cheng) summarizes the theory of X-ray standing waves (XSW), the various methods for using XSW in surface and interfaces studies, and gives a brief review of recent applications in geochemistry and mineralogy. Chapter 5 (Waychunas) covers the theory and applications of grazing-incidence X-ray absorption and emission spectroscopy, with recent examples of studies at mineral surfaces. Chapter 6 (Hirschmugl) describes the theory and applications of synchrotron infrared microspectroscopy. Chapter 7 (Manceau, Marcus, and Tamura) gives background and examples of the combined application of synchrotron X-ray microfluorescence, microdiffraction, and microabsorption spectroscopy in characterizing the distribution and speciation of metals in soils and sediments. Chapter 8 (Sutton, Newville, Rivers, Lanzirotti, Eng, and Bertsch) demonstrates a wide variety of applications of synchrotron X-ray microspectroscopy and microtomography in characterizing earth and environmental materials and processes. Finally, Chapter 9 (Myneni) presents a review of the principles and applications of soft X-ray microspectroscopic studies of natural organic materials. All of these chapters review the state of the art of synchrotron radiation applications in low temperature geochemistry and environmental science, and offer speculations on future developments. The reader of this volume will acquire an appreciation of the theory and applications of synchrotron radiation in low temperature geochemistry and environmental science, as well as the significant advances that have been made in this area in the past two decades (especially since the advent of the third-generation synchrotron sources). We hope that this volume will inspire new users to "see the light" and pursue their research using the potent tool of synchrotron radiation.
    Type of Medium: Monograph available for loan
    Pages: XXII, 579 S.
    ISBN: 0-939950-61-8 , 978-0-939950-61-4
    ISSN: 1529-6466
    Series Statement: Reviews in mineralogy & geochemistry 49
    Classification:
    Geochemistry
    Language: English
    Note: Chapter 1. An Overview of Synchrotron Radiation Applications to Low Temperature Geochemistry and Environmental Science by Gordon E. Brown, Jr. and Neil C. Sturchio, p. 1 - 116 Chapter 2. A Brief Overview of Synchrotron Radiation by T. K. Sham and Mark L. Rivers, p. 117 - 148 Chapter 3. X-ray Reflectivity as a Probe of Mineral-Fluid Interfaces: A User Guide by Paul A. Fenter, p. 149 - 220 Chapter 4. X-ray Standing Wave Studies of Minerals and Mineral Surfaces: Principles and Applications by Michael J. Bedzyk and Likwan Cheng, p. 221 - 266 Chapter 5. Grazing-incidence X-ray Absorption and Emission Spectroscopy by Glenn A. Waychunas, p. 267 - 316 Chapter 6. Applications of Storage Ring Infrared Spectromicroscopy and Reflection-Absorption Spectroscopy to Geochemistry and Environmental Science by Carol J. Hirschmugl, p. 317 - 340 Chapter 7. Quantitative Speciation of Heavy Metals in Soils and Sediments by Synchrotron X-ray Techniques by Alain Manceau, Matthew A. Marcus, and Nobumichi Tamura, p. 341 - 428 Chapter 8. Microfluorescence and MicrotomographyAnalyses of Heterogeneous Earth and Environmental Materials by Stephen R. Sutton, Paul M. Bertsch, Matthew Newville, Mark Rivers, Antonio Lanzirotti and Peter Eng, p. 429 - 484 Chapter 9. Soft X-ray Spectroscopy and Spectromicroscopy Studies of Organic Molecules in the Environment by Satish C. B. Myneni, p. 485 - 579
    Location: Reading room
    Branch Library: GFZ Library
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  • 2
    Description / Table of Contents: This volume was produced in response to the need for a comprehensive introduction to the continually evolving state of the art of synchrotron radiation applications in low-temperature geochemistry and environmental science. It owes much to the hard work and imagination of the devoted cadre of sleep-deprived individuals who blazed a trail that many others are beginning to follow. Synchrotron radiation methods have opened new scientific vistas in the earth and environmental sciences, and progress in this direction will undoubtedly continue. The organization of this volume is as follows. Chapter 1 (Brown and Sturchio) gives a fairly comprehensive overview of synchrotron radiation applications in low temperature geochemistry and environmental science. The presentation is organized by synchrotron methods and scientific issues. It also has an extensive reference list that should prove valuable as a starting point for further research. Chapter 2 (Sham and Rivers) describes the ways that synchrotron radiation is generated, including a history of synchrotrons and a discussion of aspects of synchrotron radiation that are important to the experimentalist. The remaining chapters of the volume are organized into two groups. Chapters 3 through 6 describe specific synchrotron methods that are most useful for single-crystal surface and mineral-fluid interface studies. Chapters 7 through 9 describe methods that can be used more generally for investigating complex polyphase fine-grained or amorphous materials, including soils, rocks, and organic matter. Chapter 3 (Fenter) presents the elementary theory of synchrotron X-ray reflectivity along with examples of recent applications, with emphasis on in situ studies of mineral-fluid interfaces. Chapter 4 (Bedzyk and Cheng) summarizes the theory of X-ray standing waves (XSW), the various methods for using XSW in surface and interfaces studies, and gives a brief review of recent applications in geochemistry and mineralogy. Chapter 5 (Waychunas) covers the theory and applications of grazing-incidence X-ray absorption and emission spectroscopy, with recent examples of studies at mineral surfaces. Chapter 6 (Hirschmugl) describes the theory and applications of synchrotron infrared microspectroscopy. Chapter 7 (Manceau, Marcus, and Tamura) gives background and examples of the combined application of synchrotron X-ray microfluorescence, microdiffraction, and microabsorption spectroscopy in characterizing the distribution and speciation of metals in soils and sediments. Chapter 8 (Sutton, Newville, Rivers, Lanzirotti, Eng, and Bertsch) demonstrates a wide variety of applications of synchrotron X-ray microspectroscopy and microtomography in characterizing earth and environmental materials and processes. Finally, Chapter 9 (Myneni) presents a review of the principles and applications of soft X-ray microspectroscopic studies of natural organic materials. All of these chapters review the state of the art of synchrotron radiation applications in low temperature geochemistry and environmental science, and offer speculations on future developments. The reader of this volume will acquire an appreciation of the theory and applications of synchrotron radiation in low temperature geochemistry and environmental science, as well as the significant advances that have been made in this area in the past two decades (especially since the advent of the third-generation synchrotron sources). We hope that this volume will inspire new users to "see the light" and pursue their research using the potent tool of synchrotron radiation.
    Pages: Online-Ressource (XXII, 579 Seiten)
    ISBN: 0939950618
    Language: English
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  • 3
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 78 (2001), S. 3208-3210 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The melting behavior of indium at high pressure has been studied in an externally heated diamond anvil cell (DAC) using x-ray diffraction measurements. Melting at high pressure was identified by the appearance of diffuse scattering from the melt with the simultaneous disappearance of crystalline diffraction signals. The observed melting curve is in good agreement with previous determinations based on resistivity measurements in a piston cylinder apparatus. These results demonstrate the successful melting experiments in a DAC using the x-ray diffuse scattering as the melting criterion. © 2001 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 4
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: We describe a laser heated diamond anvil cell system at the GeoSoilEnviroCARS sector at the Advanced Photon Source. The system can be used for in situ x-ray measurements at simultaneously ultrahigh pressures (to 〉150 GPa) and ultrahigh temperatures (to 〉4000 K). Design goals of the laser heating system include generation of a large heating volume compared to the x-ray beam size, minimization of the sample temperature gradients both radially and axially in the diamond anvil cell, and maximization of heating stability. The system is based on double-sided laser heating technique and consists of two Nd:YLF lasers with one operating in TEM00 mode and the other in TEM01* mode, optics to heat the sample from both sides, and two spectroradiometric systems for temperature measurements on both sides. When combined with an x-ray microbeam (3–10 μm) technique, a temperature variation of less than 50 K can be achieved within an x-ray sampled region for longer than 10 min. The system has been used to obtain in situ structural data and high temperature equations of state on metals, oxides, and silicates to 3500 K and 160 GPa. © 2001 American Institute of Physics.
    Type of Medium: Electronic Resource
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  • 5
    Publication Date: 2001-01-01
    Print ISSN: 0034-6748
    Electronic ISSN: 1089-7623
    Topics: Electrical Engineering, Measurement and Control Technology , Physics
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  • 6
    Publication Date: 2003-06-01
    Print ISSN: 0034-6748
    Electronic ISSN: 1089-7623
    Topics: Electrical Engineering, Measurement and Control Technology , Physics
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  • 7
    Publication Date: 2004-05-04
    Print ISSN: 0031-9007
    Electronic ISSN: 1079-7114
    Topics: Physics
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  • 8
    Publication Date: 2002-08-19
    Print ISSN: 0003-6951
    Electronic ISSN: 1077-3118
    Topics: Physics
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  • 9
    Publication Date: 2001-05-21
    Print ISSN: 0003-6951
    Electronic ISSN: 1077-3118
    Topics: Physics
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  • 10
    Publication Date: 2002-03-04
    Print ISSN: 0163-1829
    Electronic ISSN: 1095-3795
    Topics: Physics
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