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  • 1
    Publication Date: 2021-01-27
    Description: X-ray computed microtomography is an excellent tool for the three-dimensional analysis of rock microstructure. Digital images are acquired, visualized, and processed to identify and measure several discrete features and constituents of rock samples, by means of mathematical algorithms and computational methods. In this paper, we present digital images of volcanic rocks collected with X-ray computed microtomography techniques and studied by means of a software library, called Pore3D, custom-implemented at the Elettra Synchrotron Light Laboratory of Trieste (Italy). Using the Pore3D software, we analyzed the fabrics and we quantified the characteristics of the main constituents (vesicles, crystals, and glassy matrix) of four different types of pyroclasts: frothy pumice, tube pumice, scoria, and “crystalline” scoria. We identified the distinctive features of these different types of volcanic rocks. The frothy pumices show vesicles that coalesce in isotropic aggregates, especially toward the sample interior, while the scoriae have a low porosity and an abundance of isolated vesicles. In the “crystalline” scoria sample most of the vesicle separation is due to the presence of crystals of different types, while the tube pumice shows an anisotropic distribution of vesicles and crystals at the microscale, as also observed at the scale of the hand sample. Quantitative analysis and textural information may supply an additional tool to investigate the eruptive processes and the origin of volcanic rocks.
    Description: Published
    Description: 793-804
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: X-ray tomography ; 3D imaging ; volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 2
    Publication Date: 2017-04-04
    Description: We performed a series of X-ray tomographic experiments and lattice Boltzmann permeability simulations on pyroclastic products from explosive activity at Stromboli between December 2004 and May 2006. We reconstructed the 3-D textures of vesicles to investigate the relationship between the nature of vesiculation in the erupted products and the dynamics of gas transport in the shallow conduit in order to derive implications for the eruptive behavior of basaltic volcanoes. Scoriae from normal Strombolian explosions display remarkably consistent vesicle volume distributions fit by power laws with an exponent of 1 (±0.2). We ascribe the origin of such distributions to the combined effect of coalescence and continuous nucleation events in the steady state, shallow magma system that supplies normal Strombolian activity. Volume distributions and textures of vesicles in pumice clasts from the 5 April 2003 and 15 March 2007 paroxysmal activity are markedly different from those in the scoriae. Besides a power law function with a higher exponent, portions of these distributions can be also fit by an exponential function, suggesting the attempt of the system to reach near-equilibrium conditions. The investigated pumice clasts also lack the large, connecting vesicles responsible for the development of degassing pathways in the Stromboli magma that erupts the scoriae. This testifies to a decreased degassing efficiency of the magma associated with paroxysmal explosions and potential overpressure buildup at depth. By comparison with degassing experiments on basaltic melts, we derive a time constraint on the order of minutes to hours for the incubation of paroxysms at Stromboli.
    Description: Published
    Description: B01206
    Description: 1.5. TTC - Sorveglianza dell'attività eruttiva dei vulcani
    Description: JCR Journal
    Description: reserved
    Keywords: basaltic explosions ; vesicle textures ; third dimension ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 3
    Publication Date: 2017-04-04
    Description: We investigated the dynamics of explosive activity at Mt. Etna between 31 August and 15 December 2006 by combining vesicle studies in the erupted products with measurements of the gas composition at the active, summit crater. The analysed scoria clasts present large, connected vesicles with complex shapes and smaller, isolated, spherical vesicles, the content of which increases in scoriae from the most explosive events. Gas geochemistry reports CO2/SO2 and SO2/HCl ratios supporting a deep-derived gas phase for fire-fountain activity. By integrating results from scoria vesiculation and gas analysis we find that the highest energy episodes of Mt. Etna activity in 2006 were driven by a previously accumulated CO2-rich gas phase but we highlight the lesser role of syn-eruptive vesicle nucleation driven by water exsolution during ascent. We conclude that syn-eruptive vesiculation is a common process in Etnean magmas that may promote a deeper conduit magma fragmentation and increase ash formation.
    Description: Published
    Description: 265-269
    Description: 1.5. TTC - Sorveglianza dell'attività eruttiva dei vulcani
    Description: JCR Journal
    Description: reserved
    Keywords: Etna ; fire-fountains ; vesicle textures ; volcanic degassing ; 04. Solid Earth::04.08. Volcanology::04.08.01. Gases ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 4
    Publication Date: 2017-04-04
    Description: A series of computer microtomography experiments are reported which were performed by using a third-generation synchrotron radiation source on volcanic rocks from various active hazardous volcanoes in Italy and other volcanic areas in the world. The applied technique allowed the internal structure of the investigated material to be accurately imaged at the micrometer scale and three-dimensional views of the investigated samples to be produced as well as three-dimensional quantitative measurements of textural features. Thegeometryof thevesicle (gas-filledvoid) network in volcanic products of both basaltic and trachytic compositions were particularly focused on, as vesicle textures are directly linked to the dynamics of volcano degassing. This investigation provided novel insights into modes of gas exsolution, transport and loss in magmas that were not recognized in previous studies using solely conventional two- dimensional imaging techniques. The results of this study are important to understanding the behaviour of volcanoes and can be combined with other geosciences disciplines to forecast their future activity.
    Description: In press
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: high-resolution three-dimensional imaging ; X-ray computed microtomography ; volcanic eruptions ; volcanic rock textures ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 5
    Publication Date: 2017-04-04
    Description: Vesicle size distributions in two and three dimensions of two samples were independently measured by three different researchers to investigate whether or not such measurements are reproducible. Additionally, two different software programs were used to measure the three-dimensional vesicle size distributions: the 3D Object Counter plugin for ImageJ and Blob3D. Manual thresholding by each of the authors produced similar results for both samples using both programs; however, use of the automatic, maximum entropy technique for thresholding produced measurably different results because it did not discriminate between vesicles and plagioclase crystals in one case and between vesicles and some cracks in another. Use of asymmetric erosion and dilation processes on the images is shown to affect the vesicle size distribution, but it does not have a significant effect on the power-law exponent that describes intermediate-sized vesicles or on the vesicle number density in these samples. However, such a technique is not recommended.
    Description: Published
    Description: 70-78
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: Volcanic rocks ; vesicle counting ; reproducibility ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 6
    Publication Date: 2017-04-04
    Description: In the texture analysis of volcanic rocks, the preferred orientation of the constituents can provide useful information for the interpretation of the processes involved in the rock formation. We present here a new data analysis technique, based on X-ray microtomography measurements and on shape preferred orientation analysis, to obtain the orientation distribution functions of the constituents of volcanic rocks. This procedure proved to be very suitable for volcanic samples, where diffraction-based techniques, developed for crystallographic preferred orientation studies, are of limited utilization, in addition to the fact that they cannot provide any information about vesicles or bubbles. Moreover the analysis performed directly in three dimensions (3D) overcomes the problems that usually occur when employing stereological methods for the analysis of the images obtained via microscopy-based techniques. In this study, two scoriae (from Stromboli and Etna) and a tube pumice (from Campi Flegrei) were measured via X-ray microtomography and then the resulting volumes were analyzed following the proposed procedure. Results highlight little preferred orientation for the vesicles in the two scoria samples, whereas the pumice shows a marked preferred orientation. Crystals (also divided by mineral species) were taken into account as well and in the two scoria samples there is no crystal preferred orientation, in contrast with the pumice, where crystal preferred orientation features are very similar to the ones found for the vesicles. Overall we found strong differences in preferred orientation: weak for vesicles in scoriae, showing an axial symmetry with the axis parallel to the elongation axis of the sample, and a stronger and more complex orientation texture in the pumice sample for both crystals and vesicles. The promising results obtained suggest that this procedure is potentially very useful for the analysis of preferred orientation in volcanic rocks and geomaterials in general.
    Description: Published
    Description: 83-95
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: X-ray computed microtomography ; preferred orientation ; texture analysis ; volcanic scoria ; synchrotron X-rays ; pumice ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 7
    Publication Date: 2017-04-04
    Description: No abstract
    Description: Published
    Description: 468-469
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: Geomaterials ; 3D imaging ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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  • 8
    Publication Date: 2017-04-04
    Description: A series of computed microtomography experiments are reported which were performed by using a third-generation synchrotron radiation source on volcanic rocks from various active hazardous volcanoes in Italy and other volcanic areas in the world. The applied technique allowed the internal structure of the investigated material to be accurately imaged at the micrometre scale and three-dimensional views of the investigated samples to be produced as well as three-dimensional quantitative measurements of textural features. The geometry of the vesicle (gas-filled void) network in volcanic products of both basaltic and trachytic compositions were particularly focused on, as vesicle textures are directly linked to the dynamics of volcano degassing. This investigation provided novel insights into modes of gas exsolution, transport and loss in magmas that were not recognized in previous studies using solely conventional two-dimensional imaging techniques. The results of this study are important to understanding the behaviour of volcanoes and can be combined with other geosciences disciplines to forecast their future activity.
    Description: Published
    Description: 215-221
    Description: 2.3. TTC - Laboratori di chimica e fisica delle rocce
    Description: JCR Journal
    Description: reserved
    Keywords: high-resolution three-dimensional imaging ; X-ray computed microtomography ; volcanic eruptions ; volcanic rock textures ; 04. Solid Earth::04.08. Volcanology::04.08.05. Volcanic rocks ; 04. Solid Earth::04.08. Volcanology::04.08.07. Instruments and techniques
    Repository Name: Istituto Nazionale di Geofisica e Vulcanologia (INGV)
    Type: article
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