ISSN:
1612-1112
Keywords:
Column liquid chromatography
;
Prostaglandins
;
C18 Solid phase extraction
;
Radioimmunoanalysis
Source:
Springer Online Journal Archives 1860-2000
Topics:
Chemistry and Pharmacology
Notes:
Summary The aim of this study has been the evaluation of an automated system for on-line sample preparation using solid phase extraction and HPLC purification for the measurement of prostanoids in urine. We have established the optimum precolumn and column conditions for this analysis. The manual extraction —HPLC procedure furnishes lower recoveries and higher coefficients of variation than those obtained by the automated on-line procedure. The automated system has been applied to prostanoid analysis of human urine samples from subjects exposed to lead.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF02263832
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