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  • 1995-1999  (44)
  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 68 (1997), S. 1510-1513 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: Thermal conductivity of nickel and gold films on quartz (thickness 0.4–8 μm) was measured by a modulated thermoreflectance technique recording the surface temperature profile. Model calculations predict an optimum frequency for measuring thermal transport within the film. Measurements on films with various thicknesses reveal a thermal conductivity close to the bulk value for nickel while gold films exhibit a reduced conductivity with decreasing film thickness. © 1997 American Institute of Physics.
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 80 (1996), S. 4928-4933 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Surfaces of fluoride crystals, fractured by a single excimer laser pulse and then covered by a thin conductive layer, are imaged by scanning electron microscopy in the low-voltage secondary electron mode. As a result of charging, at lower primary electron energies a contrast enhancement can be obtained for surface fragments that are no longer tightly attached to the crystal. This differs from high-energy ((approximately-greater-than)10 keV) imaging which only yields topographic contrasts and allows the analysis of the fractured structure by edge and shadowing effects. Even contrast inversion from positive to negative charging of an entire fragment can be achieved, depending on the primary electron energy. It is shown that this effect can be utilized to discriminate between fragments with a good mechanical contact to the bulk and partially detached ones by systematically studying the contrast as a function of electron energy and specimen inclination. © 1996 American Institute of Physics.
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  • 3
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 80 (1996), S. 2013-2018 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The thermoreflectance technique is applied for imaging electric current distributions and thermal transfer in a temperature reference resistor heated by an alternating current. High-frequency scans (30 kHz) allow imaging of the current density distribution in conducting strips of the resistor while scans of amplitude and phase of the surface temperature variation at lower frequencies reveal plane, cylindrical, and spherical thermal waves. We investigate wave dimensionality as a function of heating geometry and thermal length, and present a simple method allowing a quantitative thermal analysis by exploiting the phase profile of cylindrical thermal waves. © 1996 American Institute of Physics.
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  • 4
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 78 (1995), S. 5266-5269 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A simple dispersion equation for surface thermal waves propagating along a solid surface covered with a thin film of higher thermal conductivity is presented. It is shown to describe well phase measurements with a photothermal microscope carried out on metal films on glass substrates. © 1995 American Institute of Physics.
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  • 5
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 81 (1997), S. 2966-2972 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: A photothermal microscope that provides micrometer lateral and submicrometer depth resolution was designed. Thermal conductivity measurements with modulation frequencies up to 12 MHz on single grains in polycrystalline diamond demonstrate its lateral resolution power even for a highly conducting material. Measured conductivities strongly depend on the averaged volume and values up to 2200 W/mK are found in the high frequency limit where the properties inside a grain are sampled. The capability of the instrument to measure thermal parameters on thin films is demonstrated for gold films evaporated on quartz with a thickness ranging from 20 to 1500 nm. Measurements reveal a strong thickness dependence for both thin film conductivity and the contact resistance between film and substrate. Thermal conductivity decreases monotonically from 230 to 30 W/mK whereas the contact resistance rises from 2×10−7 to 8×10−6 m2K/W with decreasing film thickness. © 1997 American Institute of Physics.
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  • 6
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 66 (1995), S. 320-322 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Metal colloids in CaF2 created by low energy electron irradiation are identified by their optical absorption bands. A mean colloid radius of 18 nm is deduced from a narrow colloid band found in crystals irradiated at room temperature. Absorption data reveal a strong influence of crystal temperature during irradiation on metallization efficiency, mean colloid size, and colloid size distribution. A reversible absorption band shift is observed when turning the electron beam on and off, which may indicate a decrease of colloid size during electron irradiation. © 1995 American Institute of Physics.
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  • 7
    Electronic Resource
    Electronic Resource
    Woodbury, NY : American Institute of Physics (AIP)
    Applied Physics Letters 73 (1998), S. 756-758 
    ISSN: 1077-3118
    Source: AIP Digital Archive
    Topics: Physics
    Notes: Local thermal conductivity inside grains of high-quality polycrystalline diamond grown by chemical vapor deposition is measured at room temperature with micrometer spatial resolution. An effective conductivity is determined by choosing experimental conditions where the measured heat flow extends over adjacent grains. It is found that the effective conductivity may vary by a factor of 2, depending on the averaged volume and position on the sample. These variations are attributed to different grain structures present at the investigated locations. Local conductivity within a single grain varies by ±30% and a maximum value of 2350 W/mK is found. Local thermal conductivity data are related to the crystalline quality and impurity content determined by micro-Raman measurements. © 1998 American Institute of Physics.
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  • 8
    Electronic Resource
    Electronic Resource
    Springer
    Applied physics 62 (1996), S. 493-497 
    ISSN: 1432-0649
    Keywords: 66.70. + f
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract We investigated the anisotropic thermal conductivity in pyrolytic graphite by thermoreflectance. A laser-heated circular spot on a surface perpendicular to the planes developed into an elliptical temperature distribution which was recorded by a raster scanning technique at modulation frequencies ranging from 600 Hz to 100 kHz. The ratio of in-plane and perpendicular thermal conductivity was determined by fitting the phase of the temperature data with an analytical model, and was found to decrease with increasing modulation frequency. Highest conductivity values were considerably smaller than previously published data based on steady-state measurements. The frequency dependence and additional features in the phase profiles at high frequencies are discussed in view of sample surface preparation and the local nature of the thermoreflectance measurement.
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  • 9
    ISSN: 1432-0630
    Keywords: PACS: 79.20.-Ds; 81.65.-b
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract. Ablation thresholds and damage behavior of cleaved and polished surfaces of CaF2, BaF2, LiF and MgF2 subjected to single-shot irradiation with 248 nm/14 ns laser pulses have been investigated using the photoacoustic mirage technique and scanning electron microscopy. For CaF2, standard polishing yields an ablation threshold of typically 20 J/cm2. When the surface is polished chemo-mechanically, the threshold can be raised to 43 J/cm2, while polishing by diamond turning leads to intermediate values around 30 J/cm2. Cleaved surfaces possess no well-defined damage threshold. When comparing different fluoride surfaces prepared by diamond turning it is found that the damage resistivity roughly scales with the band gap. We find an ablation threshold of 40 J/cm2 for diamond turned LiF while the MgF2 surface can withstand a fluence of more than 60 J/cm2 without damage. The damage topography of conventionally polished surfaces shows flaky ablation across the laser-heated area with cracks along the cleavage planes. No ablation is observed in the case of chemo- mechanical polishing; only a few cracks appear. Diamond turned surfaces show small optical absorption but mostly cracks and ablation of flakes and, in some cases, severe damage in the form of craters larger than the irradiated area. The origin of such different damage behavior is discussed.
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  • 10
    ISSN: 1432-0649
    Keywords: PACS: 77.84.-s; 78.20.-e; 78.47.+p; 78.60.-b; 79.20.Ds
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: 3 following excitation with 248 nm/14 ns laser pulses at room temperature for the two Ce concentrations 0.03 and [%mol]1. The relative intensities of the 5d-4f bands emitted from Ce3+ at regular and at perturbed lattice sites were found to vary linearly with time for the higher concentration and quadratically for the lower one. This can be explained by radiative energy transfer between the two sites and generation of new perturbed sites at a rate that only shows up for the low Ce concentration. Lifetimes of the respective emission bands were determined to be about 18 ns and 41 ns. Despite resonant absorption of the 5 eV photons, surprisingly high ablation thresholds – 16 J/cm2 for 0.03% Ce, and 10 J/cm2 for 1% Ce – were observed by the probe-beam deflection technique. The reason is the strong energy loss due to intense fluorescence and deposition of the nonradiative energy fraction in the bulk rather than at the surface. The depth of energy deposition was revealed by scanning electron microscopy in the form of distinctly different ablation morphologies for the two Ce concentrations.
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